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Icap 6000 series icp

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The ICAP 6000 Series ICP is an inductively coupled plasma (ICP) spectrometer used for elemental analysis. It is designed to accurately determine the concentration of trace elements in a wide range of sample types. The ICAP 6000 Series ICP utilizes advanced optical and electronics technology to provide rapid, high-precision measurements.

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ICAP 6000 (84 citations) ICAP 6000 series (73 citations) ICAP 6000 series ICP-OES (2 citations) ICAP 6000 Series ICP Emission Spectrometer (2 citations) ICAP 6000 Series ICP-OES Spectrometer (2 citations)

4 protocols using icap 6000 series icp

1

Measuring Glass Fiber Elemental Composition

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The composition of the glass fibres and particles was measured by Inductively Coupled Plasma Optical Emission Spectroscopy (ICP-OES) (Thermo Scientific, iCAP6000 Series ICP). 100 mg of glass fibres or particles were mixed with 400 mg lithium metaborate (Alfa Aesar) and heated to 950°C for 30 min in a platinum crucible to form a fused pellet. Once cooled, the pellet was dissolved in 50 ml of 2 M HNO3. This was diluted 1:10 and ICP-OES used to measure the elemental concentration of the solution, and the composition calculated.
Solanki A.K., Autefage H., Rodriguez A.R., Agarwal S., Penide J., Mahat M., Whittaker T., Nommeots-Nomm A., Littmann E., Payne D.J., Metcalfe A.D., Quintero F., Pou J., Stevens M.M, & Jones J.R. (2023). Cobalt containing glass fibres and their synergistic effect on the HIF-1 pathway for wound healing applications. Frontiers in Bioengineering and Biotechnology, 11, 1125060.
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2

Quantification of Pd and S in PdNPs

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About 5 mg of each PdNP sample was fully digested in about 0.5 mL of aqua regia. Each sample was diluted with water to 250 mL. Standard dilutions (100, 50, 20, 10, 5, 2, 1, 0.5, and 0.1 ppm) for palladium and sulfur were prepared. ICP-AES data for palladium (229.651 nm) and sulfur (180.731 nm) were obtained by using Thermo Scientific ICAP 6000 Series ICP emission spectrometers. Standard curves for palladium and sulfur were constructed and used to determine the relative abundance of palladium and sulfur in the PdNP samples.
Vargas K.M., San K.A, & Shon Y.S. (2019). Isolated Effects of Surface Ligand Density on the Catalytic Activity and Selectivity of Palladium Nanoparticles. ACS applied nano materials, 2(11), 7188-7196.
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3

Determining Ca, Sr, and Ba Concentrations

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Concentrations of Ca and Sr were measured on an inductively coupled plasma (ICP) atomic emission spectrometer (iCAP 6000 Series ICP, Thermo Fisher Scientific), and concentrations of Sr and Ba were measured on an inductively coupled plasma mass spectrometer (ICP-MS; 7500 CX, Agilent) following the procedure given by Balter and Lécuyer (35 ).
Tacail T., Martin J.E., Arnaud-Godet F., Thackeray J.F., Cerling T.E., Braga J, & Balter V. (2019). Calcium isotopic patterns in enamel reflect different nursing behaviors among South African early hominins. Science Advances, 5(8), eaax3250.
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4

Comprehensive Water Quality Analysis

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The pH values of surface water and pore water samples were measured using a combined pH electrode with a Ag/AgCl internal reference (Orion Research, Beverly, CA, USA) and a TIM800 pH meter. Turbidity was measured using a Turb 550 turbidity meter (WTW GmbH, Weilheim). Total dissolved inorganic carbon concentrations were measured using infrared gas analysis (IRGA, ABB Advance Optima, Zu ¨rich, Switzerland). Prior to elemental analyses, 10 ml of each sample was stored at 4 °C until analyses with 0.1 ml (65 %) HNO À 3 to prevent metal precipitation. For the analyses of P, Ca, Mg, Fe, S, K and Al inductively coupled plasma spectrophotometry (ICP-Optical Emission Spectrometer, Thermo Scientific iCAP 6000 Series ICP) was used. To determine nitrate (Kamphake et al. 1967) , ammonium (Grasshoff and Johanssen 1972) , orthophosphate (Henriksen 1965) , sodium and chloride concentrations, 20 ml of each sample was stored at -20 °C and analyzed colorimetrically with an Auto Analyzer 3 system (Bran and Luebbe). Sodium and potassium were determined with a Technicon Flame Photometer IV Control (Technicon Corporation).
van Dijk G., Smolders A.J.P., Loeb R., Bout A., Roelofs J.G.M, & Lamers L.P.M. (2015). Salinization of coastal freshwater wetlands; effects of constant versus fluctuating salinity on sediment biogeochemistry. Biogeochemistry., 126(1-2).
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