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Titanium 4 isopropoxide ti oipr 4

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Titanium(IV) isopropoxide (Ti(OiPr)4) is a colorless, volatile liquid. It is a metal-organic compound that serves as a precursor for the deposition of titanium dioxide thin films and nanoparticles.

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Lab products found in correlation

Methanol ch3oh, by Xilong (3 mentions) Acetophenone, by Merck Group (1 mentions) Magnesium acetate tetrahydrate, by Merck Group (1 mentions) Calcium nitrate tetrahydrate, by Thermo Fisher Scientific (1 mentions) Zirconyl chloride octahydrate, by Thermo Fisher Scientific (1 mentions) Pluronic p123 eo20po70eo20, by Merck Group (1 mentions) Cobalt 2 nitrate hexahydrate, by Merck Group (1 mentions) Tetraethyl orthosilicate teos, by Merck Group (1 mentions) Sodium chloride (nacl), by Merck Group (1 mentions) Cobalt 2 chloride hexahydrate cocl2 6h2o, by Thermo Fisher Scientific (1 mentions) Squalane, by Thermo Fisher Scientific (1 mentions) Toluene, by Merck Group (1 mentions) Acetic anhydride, by Merck Group (1 mentions)

4 protocols using titanium 4 isopropoxide ti oipr 4

1

Titanium Isopropoxide-Assisted Synthesis

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Titanium(IV) isopropoxide (Ti(OiPr)4, 97 %), and acetophenone (99%) were obtained from Sigma-Aldrich. Diethyl 1-octylphosphonate (C8H17PO3Et2, 98%) was purchased from Sikémia. Toluene was dried over a Pure-Solve MD5 solvent purification system (H2O <10 ppm, controlled with a Karl Fischer coulometer). All other chemicals were used without further purification. All manipulations were carried out in a glove box under argon atmosphere (<5 ppm of water and O2).
Wang Y., Mutin P.H, & Alauzun J.G. (2019). One-step nonhydrolytic sol–gel synthesis of mesoporous TiO2 phosphonate hybrid materials. Beilstein Journal of Nanotechnology, 10, 356-362.
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2

Synthesis of Inorganic Composite Materials

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Pluronic P123 (EO20:PO70:EO20, Mn = 5800, Sigma-Aldrich),
tetraethyl orthosilicate (TEOS; reagent grade 98%, Sigma-Aldrich),
HCl (37–38%, J.T. Baker), magnesium acetate tetrahydrate (MgAc2·4H2O; ACS reagent grade 99%, Sigma-Aldrich),
aluminum isopropoxide (Al(−OiPr)3; ≥98%, Sigma-Aldrich), calcium nitrate tetrahydrate
(Ca(NO3)2·4H2O; 99%, Alfa Aesar),
titanium(IV) isopropoxide (Ti(−OiPr)4; 97%, Sigma-Aldrich), zirconyl chloride octahydrate
(ZrOCl2·8H2O; ≥98%, Acros Organics),
sodium chloride (NaCl; ACS reagent grade ≥99.0%, Sigma-Aldrich),
and cobalt(II) nitrate hexahydrate (Co(NO3)2·6H2O; ACS reagent grade 99.5%, Sigma-Aldrich) were
used as purchased.
Belthle K.S., Beyazay T., Ochoa-Hernández C., Miyazaki R., Foppa L., Martin W.F, & Tüysüz H. (2022). Effects of Silica Modification (Mg, Al, Ca, Ti, and Zr) on Supported Cobalt Catalysts for H2-Dependent CO2 Reduction to Metabolic Intermediates. Journal of the American Chemical Society, 144(46), 21232-21243.
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3

Synthesis of Metal-Organic Frameworks

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Titanium (IV) isopropoxide (Ti(OiPr)4) and 2-amino terephthalic acid (H2NC6H3-1,4-(CO2H)2) were purchased from Sigma-Aldrich Co. (St. Louis, MO, USA). Iron(III) chloride hexahydrate (FeCl3·6H 2O), nickel chloride hexahydrate (NiCl2·6H2O), and cobalt(II) chloride hexahydrate (CoCl2·6H2O) were obtained from Fisher Scientific (Fair Long, NJ, USA). N-dimethylformamide (DMF, 99.5%) and methanol (CH3OH) were bought from Xilong Chemical Co., Ltd. (Guangdong, China).
Nguyen Thi H.T., Tran Thi K.N., Hoang N.B., Tran B.T., Do T.S., Phung C.S, & Nguyen Thi K.O. (2021). Enhanced Degradation of Rhodamine B by Metallic Organic Frameworks Based on NH2-MIL-125(Ti) under Visible Light. Materials, 14(24), 7741.
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4

Synthesis of Titanium Oxide Nanoparticles

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All manipulations were carried out in a glovebox under argon atmosphere (<10 ppm of water and O2). Titanium (IV) isopropoxide (Ti(O i Pr)4, 97%) and acetic anhydride (Ac2O, 99%) were obtained from Sigma-Aldrich and were used without further purification. Squalane (98%) was purchased from Alfa Aesar. Commercial titanium oxide nanoparticles (labeled TiO2-Comm in the following) were purchased from Tronox (AK-1, anatase, SBET = 85 m 2 g -1 , average crystallite size 17.5 nm). Toluene (Sigma-Aldrich, 99.7%) was dried over a PureSolve MD5 solvent purification system (H2O <10 ppm, controlled with a Karl Fischer coulometer).
Wang Y., Kim S., Louvain N., Alauzun J.G, & Mutin P.H. (2019). Acetic Anhydride as an Oxygen Donor in the Non-Hydrolytic Sol-Gel Synthesis of Mesoporous TiO2 with High Electrochemical Lithium Storage Performances. Chemistry (Weinheim an der Bergstrasse, Germany), 25(18).
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