Tga sdta851e system
The TGA/SDTA851e system is a thermogravimetric analysis (TGA) and simultaneous differential thermal analysis (SDTA) instrument. It is designed to measure changes in the weight of a sample as a function of temperature or time in a controlled atmosphere. The instrument can be used to characterize the thermal stability, composition, and decomposition behavior of various materials.
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4 protocols using tga sdta851e system
Multimodal Characterization of Nanomaterials
Thermal Transition of PHB Extraction
Characterization of LDH Materials
characterized by PXRD using a Bruker D8 ADVANCE powder diffractometer
(source Cu Kα radiation, Ni filter, λ = 1.5418 Å)
operating in reflection geometry. The PXRD patterns of the LDHs were
indexed by using APPLEMAN program, part of the code PROSZKI suite
of programs. The PXRD patterns of the oxide residues were indexed
by “finger printing” by comparing the observed 2θ
values with those reported in the powder diffraction files. TGAs were
carried out using a Mettler Toledo TGA/SDTA 851e system
(25–900 °C, heating rate 5 °C min–1) driven by STARe 7.01 software. The analyses were carried
out in flowing N2 (control) and flowing CO2 (test)
to measure the mass gain if any, as a result of CO2 uptake.
In separate experiments, the LDHs were heated in the TGA balance at
different temperatures determined by the appearance of plateaus in
the TGA profile. The phases obtained were analyzed by PXRD. TGA measurements
were also carried out on CaO and Ca(OH)2 used as controls.
IR spectra were recorded by using a Bruker model Alpha-P IR spectrometer
(Diamond ATR cell, 400–4000 cm–1, 4 cm–1 resolution).
Thermogravimetric Analysis of Nanoemulsions
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