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Ferrocene fc

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Ferrocene (Fc) is an organometallic compound consisting of two cyclopentadienyl rings bound to an iron center. It is a versatile compound used in various applications, including as a reference material in electrochemical studies and as a precursor for the synthesis of other organometallic compounds.

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Lab products found in correlation

Tetrabutylammonium hexafluorophosphate tbapf6, by Merck Group (2 mentions) Methanol, by Merck Group (2 mentions) Acetonitrile, by Merck Group (2 mentions) Dimethyl sulfoxide (dmso), by Thermo Fisher Scientific (1 mentions) Anthraquinone, by Merck Group (1 mentions) Toluene, by Merck Group (1 mentions) Oleylamine, by Merck Group (1 mentions) Copper chloride, by Merck Group (1 mentions) Tetrabutylammonium perchlorate tba clo4, by Merck Group (1 mentions) Tetrachloroethylene tce, by Merck Group (1 mentions) 1 octadecene ode, by Merck Group (1 mentions) Sulfur powder, by Thermo Fisher Scientific (1 mentions) Toluene, by Thermo Fisher Scientific (1 mentions) Anhydrous dimethyl sulfoxide, by Merck Group (1 mentions) Hydrochloric acid (hcl), by Merck Group (1 mentions) 1 octadecanethiol, by Merck Group (1 mentions) Copper 2 acetate monohydrate, by Merck Group (1 mentions) 16 mercaptohexadecanoic acid, by Merck Group (1 mentions) Tetrabutylammonium tetrafluoroborate tbatfb, by Merck Group (1 mentions) 11 mercapto 1 undecanol, by Merck Group (1 mentions)

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Ferrocene (92 citations)

13 protocols using ferrocene fc

1

Electrochemical Characterization of C60

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C60 (99.5% Sigma-Aldrich, sp. z o.o., Poznan, Poland); tetraethylammonium tetrafluoroborate (E1, 99%, Sigma-Aldrich); tetrabutylammonium tetrafluoroborate (E2, 99%, Sigma-Aldrich) dried under a vacuum; dichloromethane (DCM, HPLC, 99.8%, Sigma-Aldrich); acetonitrile (ACN, Sigma-Aldrich, 99%); Ru3(CO)12 (Sigma-Aldrich); ferrocene (Fc, 98%, Sigma-Aldrich); and argon (6.0, SIAD Group, Ruda Śląska, Poland).
Czichy M., Colombo A., Wagner P., Janasik P., Dragonetti C., Raja R., Officer D.L, & Wang L. (2021). Exohedral Functionalization of Fullerene by Substituents Controlling of Molecular Organization for Spontaneous C60 Dimerization in Liquid Crystal Solutions and in a Bulk Controlled by a Potential. Polymers, 13(16), 2816.
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2

Electrochemical Characterization of Anthraquinone Derivatives

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Anthraquinone (AQ, 97%), octafluoroAnthraquinone
(AQ-F8, 96%), 1,4-methoxyAnthraquinone (1,4-OMe-AQ, >99%),
1,4-difluoroAnthraquinone (1,4-F-AQ, 98%), ferrocene (Fc), and tetrabutylammonium
hexafluorophosphate (TBAPF6) were purchased from Sigma-Aldrich.
1-ChloroAnthraquinone (1-Cl-AQ, 98%) was purchased from Thermo Fisher
Scientific. 2-ChloroAnthraquinone (2-Cl-AQ, >99%) was purchased
from
Chemcruz Enterprises Ltd. 1-HydroxyAnthraquinone (1-OH-AQ, >95%)
was
purchased from Cayman Chemical Company. Dimethyl sulfoxide (DMSO)
was purchased from Thermo Fisher Scientific. All chemicals were used
without further purification.
Bui A.T., Hartley N.A., Thom A.J, & Forse A.C. (2022). Trade-Off between Redox Potential and the Strength of Electrochemical CO2 Capture in Quinones. The Journal of Physical Chemistry. C, Nanomaterials and Interfaces, 126(33), 14163-14172.
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3

Synthesis and Characterization of Copper-based Nanoparticles

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Copper chloride (CuCl, 98%, Sigma-Aldrich),
oleylamine (OLAM, 80%, Sigma-Aldrich), 1-octadecene (ODE, 90%, Sigma-Aldrich),
sulfur powder (S, 99.99%, Alfa Aesar), octanedithiol (ODT, 98%, Sigma-Aldrich),
Indium-doped Tin Oxide substrates (ITO, ∼25 nm film thickness, Rsq ≤ 120 Ω/cm2, PGO
Germany), lithium perchlorate (LiClO4, 99.99%, Sigma-Aldrich),
tetraoctylammonium tetrafluoroborate ((TOA)BF4, >98%,
Sigma-Aldrich),
tetrabutylammonium perchlorate ((TBA)ClO4, >98%, Sigma-Aldrich),
tetramethylammonium hexafluorophosphate ((TMA)PF6, >98%,
Sigma-Aldrich), cesium perchlorate (CsClO4, 99.995%, Sigma-Aldrich),
copper(I) tetrafluoroborate (CuBF4, >98%, Sigma-Aldrich),
ferrocene (Fc, 98%, Sigma-Aldrich). Anhydrous solvents (methanol,
99.8%, butanol, 99.8%, toluene, 99.8%, tetrachloroethylene (TCE, >99%)
and acetonitrile, 99.99%) were all purchased from Sigma-Aldrich. acetonitrile
was dried before use in an Innovative Technology PureSolv Micro column.
All other chemicals were used as received.
van der Stam W., Gudjonsdottir S., Evers W.H, & Houtepen A.J. (2017). Switching between Plasmonic and Fluorescent Copper Sulfide Nanocrystals. Journal of the American Chemical Society, 139(37), 13208-13217.
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4

Electrochemical Characterization of Ionic Liquid

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Toluene (analytical reagent grade, Fischer Scientific) and ferrocene (Fc, 98%, Sigma-Aldrich) were each used as received; trihexyltetradecylphosphonium bis(trifluoromethylsulfonyl)imide ([P6,6,6,14][NTf2], >98%) was acquired from Iolitech, Germany and used as received. The water used was ultrapure water (Millipore, resistivity = 18.2 MΩ cm) and nitrogen and oxygen were obtained from oxygen-free, BOC Gases plc. Finally carbon microfibers (diameter 7 μm) were obtained from (Goodfellow Cambridge Ltd.).
Feng A., Cheng W, & Compton R.G. (2016). Measuring the oxygen content of a single oil droplet †Electronic supplementary information (ESI) available. See DOI: 10.1039/c6sc02357f Click here for additional data file.. Chemical Science, 7(10), 6458-6462.
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5

Synthesis and Characterization of Organometallic Compounds

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1,3,5-tris(4-carboxyphenyl)benzene [BTB] (98%), 1,3,5-tris(4’carboxy[1,1᾿-biphenyl]-4-yl)benzene [BBC] (95%), copper (II) acetate monohydrate, 16-mercaptohexadecanoic acid [MHDA] (90%), 11-mercapto-1-undecanol [MUD] (97%), 1-octadecanethiol [ODT] (98%), hydrochloric acid (ACS reagent, 37%), anhydrous propylene carbonate [PC], and anhydrous dimethyl sulfoxide [DMSO] are from Sigma Aldrich (St. Louis, MO). Absolute, anhydrous ethanol (200 proof, ACS/USP Grade) was obtained from Phamco-Aaper (Shelbyville, KY). These chemicals were used as received. Ferrocene (Fc, Sigma Aldrich) and tetrabutylammonium tetrafluoroborate (TBATFB, Sigma Aldrich) were dried at 120 °C under vacuum for 12 h prior to transferring to an Ar-filled glovebox (less than 1 ppm O2/H2O). Silicon wafers with a 5 nm Ti adhesion layer and a 100 nm Au layer were obtained from Platypus Technologies (New Orleans, LA). Ge (100) wafers were obtained from MTI Corporation (Richmond, CA).
Lau J., Trojniak A.E., Maraugha M.J., VanZanten A.J., Osterbaan A.J., Serino A.C., Ohnsorg M.L., Cheung K.M., Ashby D.S., Weiss P.S., Dunn B.S, & Anderson M.E. (2019). Conformal Ultrathin Film Metal–Organic Framework Analogues: Characterization of Growth, Porosity, and Electronic Transport. Chemistry of materials : a publication of the American Chemical Society, 31(21), 8977-8986.
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6

Preparation of Ferrocene-based Reference Electrode

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The Pt|Fc/Fc+ RE was prepared
following literature procedure
with a 0.5 mm diameter Pt wire (Sigma-Aldrich), ferrocene (Fc, 98%,
Sigma-Aldrich), ferrocenium hexafluorophosphate (FcPF6,
95%, Combi-Blocks), TBAPF6, and THF.64 (link)−66 (link) Fc and TBAPF6 were recrystallized prior to use. The Pt wire, cleaned in
concentrated HNO3 and heated in a H2 flame prior
to use, was sealed within a ceramic-fritted glass tube (inner diameter
3.5 mm, Pine Research Instrumentation). The glass tube was filled
with an electrolyte of 4 mM Fc, 4 mM FcPF6, and 0.1 M TBAPF6 in THF. The RE was assembled fresh prior to each experiment.
Zhang W., Gu C., Wang Y., Ware S.D., Lu L., Lin S., Qi Y, & See K.A. (2023). Improving the Mg Sacrificial Anode in Tetrahydrofuran for Synthetic Electrochemistry by Tailoring Electrolyte Composition. JACS Au, 3(8), 2280-2290.
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7

Electrochemical Characterization of Materials

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All materials were purchased and used as received unless otherwise mentioned. Propylene carbonate (PC, 99.7%, anhydrous), tetrabutylammonium hexafluorophosphate (TBAPF6, 99%), potassium nitrate (KNO3, ACS grade, 99+%), hydroxymethylferrocene (FcMeOH, 97%), and ferrocenium hexafluorophosphate (Fc+PF6−, 97%) were purchased from Sigma. Ferrocene (Fc, 98%, Sigma) was recrystallized twice out of hexane. DI water was obtained from a Millipore ultrapure system. Grade 1 HOPG and GC were purchased from SPI supplies; GC was cut using a wire electrical discharge machine (EDM) and sonicated twice in acetone and IPA before use. C 1s XPS spectra of the revealed presence of C‐OH/C‐OR groups (Figure S22a). Cu (99.99%) and Ni (99%) foil were purchased from Alfa Aesar. 3 mm GC macro‐disc electrodes were purchased from BASi. Cu etchant (CE‐100) and Ni etchant (TFB) was procured from Transene Company Inc. Si/SiO2 wafers were purchased from University Wafer.
Gaddam R., Sarbapalli D., Howard J., Curtiss L.A., Assary R.S, & Rodríguez‐López J. (2022). An SECM‐Based Spot Analysis for Redoxmer‐Electrode Kinetics: Identifying Redox Asymmetries on Model Graphitic Carbon Interfaces. Chemistry, an Asian Journal, 18(2), e202201120.
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8

Fullerene-Peptide Derivatives Synthesis

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The fullerene–peptide derivatives 2–12 were synthesized according to the literature procedure [27 (link)]. The solvents (HPLC grade) used for the CV and SEM experiments were stored over 3 Å molecular sieves and degassed under vacuum prior to use. Ferrocene (Fc) and tetrabutylammonium perchlorate (TBAP) were purchased from Sigma-Aldrich and used as received.
Bjelaković M.S., Kop T.J., Đorđević J, & Milić D.R. (2015). Fulleropeptide esters as potential self-assembled antioxidants. Beilstein Journal of Nanotechnology, 6, 1065-1071.
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9

Synthesis of Colloidal Quantum Dots

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Copper(I) iodide (CuI, 99.999%, Sigma-Aldrich),
indium acetate (InAc3, 99.99%, Sigma-Aldrich), 1-dodecanethiol
(DDT, >98%, Sigma-Aldrich), ethanedithiol (EDT, >98%, Sigma-Aldrich),
indium-doped tin oxide substrates (ITO, ∼ 25 nm film thickness, Rsq ≤ 120 Ω/cm,2 (link) PGO Germany), thin Indium-doped tin oxide substrates (ITO,
∼25 nm film thickness, total substrate thickness of ∼100
μm, Rsq ≤ 120 Ω/cm,2 (link) PGO Germany), lithium perchlorate (LiClO4, 99.99%, Sigma-Aldrich), and ferrocene (Fc, 98%, Sigma-Aldrich)
were used. Anhydrous solvents (methanol, 99.8%; butanol, 99.8%; and
toluene, 99.8%) and acetonitrile (99.99%) were all purchased from
Sigma-Aldrich. acetonitrile was dried before use in an Innovative
Technology PureSolv Micro column. All other chemicals were used as
received.
van der Stam W., de Graaf M., Gudjonsdottir S., Geuchies J.J., Dijkema J.J., Kirkwood N., Evers W.H., Longo A, & Houtepen A.J. (2018). Tuning and Probing the Distribution of Cu+ and Cu2+ Trap States Responsible for Broad-Band Photoluminescence in CuInS2 Nanocrystals. ACS Nano, 12(11), 11244-11253.
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10

Synthesis and Characterization of Iron-Porphyrins

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All reagents were of the highest grade commercially available and were used without further purification. The iron-porphyrins (FeIIIL2(Br), FeIIIL3(Br) and FeIIITPP(Br)) studied here were synthesized according to previously reported procedures.59 (link) 3-Chloroperoxybenzoic acid (m-CPBA) was purchased from Aldrich (77%) and purified by washing with pH 7.40 phosphate buffer and recrystallized from pentane to remove 3-chlorobenzoic acid. Purity (>95%) was determined by 1H NMR. Solvents were purchased from RANKEM with HPLC grade for spectroscopic purpose. 2,4,6-Tritertiary butyl phenol (TBPH) and ferrocene (Fc) were also purchased from Sigma-Aldrich.
Bhunia S., Rana A., Dey S.G., Ivancich A, & Dey A. (2020). A designed second-sphere hydrogen-bond interaction that critically influences the O–O bond activation for heterolytic cleavage in ferric iron–porphyrin complexes. Chemical Science, 11(10), 2681-2695.
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