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Silicotungstic acid hydrate

Manufactured by Merck Group
Sourced in United Kingdom

Silicotungstic acid hydrate is a chemical compound that can be used as a laboratory reagent. It has the molecular formula H4[SiW12O40]·xH2O. The core function of this product is to serve as a chemical reagent in various analytical and experimental procedures.

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2 protocols using silicotungstic acid hydrate

1

Vanadyl Silicotungstate Synthesis in Iso-Propanol

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EXAMPLE 2

Preparation of Vanadyl Silicotungstate in iso-propanol

1.14 g of silicotungstic acid hydrate (Fluka) (0.359 mmoles) dissolved in 20 ml of iso-propanol (Aldrich) were placed in a 250 ml flask and subsequently, 116 g of vanadium(V) oxytriisopropoxide (Cas No. 5588-84-1) (Aldrich) (0.475 mmoles) dissolved in 60 ml of iso-propanol (Aldrich) were added: the mixture obtained was heated to 70° C., for 3 hours, obtaining a colorless solution. The solution obtained was cooled to ambient temperature (25° C.) and transferred into a glass vessel with a plug: one drop of said solution was placed on a strip of wet litmus paper to measure the pH, which was equal to about 6-7.

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2

Mesoporous Silica Nanoparticle Synthesis

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All reagents and solvents used in this work were purchased from commercial sources and used without further purification: Glycerol (99.92%, VWR Chemicals, Lisbon, Portugal), acetone (99.5%, Honeywell, NC, USA), methanol (99.9%, Fisher Scientific, Loughborough, UK), Pluronic P123 (Aldrich, London, UK), hydrochloric acid (HCl, 37%, Aldrich, London, UK), tetraethoxysilane (TEOS, Aldrich, London, UK), 3-aminopropyltriethoxysilane (Aptes, 98%, Aldrich, London, UK), anhydrous toluene (99.8%, Aldrich, London, UK), acetonitrile (Carlo Reba Reagents, Milano, Italy), ethanol (99.8%, Honeywell, NC, USA), phosphomolybdic acid hydrate (H3[PMo12O40].nH2O, Aldrich, London, UK), phosphotungstic acid hydrate (H3[PW12O40].nH2O, Aldrich, London, UK), and silicotungstic acid hydrate (H4[SiW12O40].nH2O, Aldrich, London, UK).
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