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3 protocols using 2 hydroxy 2 methylpropiophenone

1

Synthesis of HEMA-Based Hydrogel for Cartilage Regeneration

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2-hydroxyethyl methacrylate (HEMA), triphosgene, 2-hydroxyethyl methacrylate (HEMA), apocynin (APO), kartogenin (KGN), 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (EDC), 4-dimethylaminopyridine (DMAP), 2-Hydroxy-2-methylpropiophenone and 2, 2′-azobis (2-methylpropionitrile) (AIBN), polyethyleneglycol (PEG5000-OH) were purchased from Energy Chemical (Shanghai, China).
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2

Synthesis and Characterization of MOF Materials

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TPM (98%) and azobisisobutyronitrile (AIBN, 98%) were obtained from Sigma-Aldrich. Ammonia (28%), aluminum nitrate nonahydrate [Al(NO3)3·9H2O, 99.5%], 2-aminoterephthalic acid (NH2- H2bdc, 98%), caprylic acid (98%), and the photoinitiator, 2-hydroxy-2-methylpropiophenone (98%) were purchased from Energy Chemical. PL61 (number-average molecular weight, ~2000) was purchased from Aldrich Chemistry. 1,3,5-benzenetricarboxylic acid (H3btc, 99%), tetrabutyl titanate (TBT: 99%), SDS (99%), and rhodamine B (99%) were purchased from J&K Scientific Ltd. Zirconium (IV) oxide chloride octahydrate (ZrOCl2·8H2O, 98%), hydroquinone (99%), iron(II) chloride tetrahydrate (FeCl2·4H2O, 99%) were purchased from Dieckmann Chemicals. Iron(III) chloride hexahydrate (FeCl3·6H2O, 99%) was obtained from Alab (Shanghai) Chemical Technology Co. Ltd. The D5 dye, 3-{5-[4-(diphenylamino)styryl]thiophen-2-yl}-2-cyanoacrylic acid (>95%) was purchased from Dyenamo. Other chemicals include acetic acid (HAc; 99.7%; Chemicals Duksan), polyvinyl alcohol (98 to 99%; Alfa Aesar), benzoquinone (99%; Acros Organics), and hydrochloric acid (HCl; 37%; RCI Labscan Ltd).
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3

Ibuprofen-based Biomaterial Synthesis

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Ibuprofen, 2-hydroxyethyl methacrylate (HEMA), 1-(3-Dimethylaminopropyl)-3- ethylcarbodiimide hydrochloride (EDC), 4-dimethylaminopyridine (DMAP), 2 - Hydroxy - 2 - methylpropiophenone and 2, 2’ - azobis (2 - methylpropionitrile) (AIBN) were purchased from Energy Chemical (Shanghai, China).
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