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2 protocols using 1 3 5 triphenyl benzene

1

Synthesis and Characterization of Fluorinated Compounds

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Perfluoro tributylamine (FC 43), Perfluoro kerosene (PFK), perfluoro alkyl phosphazene (Ultramark 1621), tris(perfluoro alkylethyl) silyl alkylamine (Ultramark 3200F), 4-(1,1,3,3-tetramethylbutyl)phenyl-polyethylene glycol (Triton X-100), and polyethylene glycol (PEG 1000), ribose (C5H10O5; 150.0528 g mol−1), kaempferol (C15H10O6; 286.0477 g mol−1), 1,3,5-triphenyl benzene (C24H18; 306.1408 g mol−1) and pyrene (C16H10; 202.0783 g mol−1) were all purchased from Sigma Aldrich Chemie GmbH (Schnelldorf, Germany).
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2

Polymer Fractionation and Crude Oil Analysis

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Commercially available Torlon® 4000T-LV and Matrimid®5218 were purchased from Solvay Advanced Polymers (Alpharetta, GA) and Huntsman, respectively. SBAD-1, DUCKY-9, and DUCKY-10 polymers were synthesized from literature procedures detailed in two previous publications4 ,5 (link). Two real crude oils (Permian and Arabian light crude oils) were provided from ExxonMobil Technology and Engineering Company. The experimental results of the two fractionations were published previously4 ,5 (link). All other chemicals (p-xylylene diamine, lithium nitrate, chloroform, tetrahydrofuran, 1-methylpyrroldone, ethanol, methanol, hexane, toluene, toluene, Tert-butyl benzene, 1,3,5-triisopropyl benzene, n-Octane, iso-Octane, iso-cetane, methylcyclohexane, decalin, 1-methylnaphthalene, o-xylene, propyl benzene, mesitylene, n-butylcyclohexane, tetralin, bi-phenyl, dodecylbenzene, 1,3,5-triphenylbenzene, 1,3,5-Tris[(3-methylphenyl) phenylamino]benzene), methanol, and guaiacol were purchased from Sigma Aldrich, Alfa Aesar, or TCI and used as received.
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