Acetone d6

Manufactured by Eurisotop

Sourced in France

Acetone-d6 is a deuterated form of acetone, with all hydrogen atoms replaced by deuterium. It is a colorless, volatile liquid commonly used as a solvent and reagent in various laboratory applications.

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5 protocols using acetone d6

NMR Spectroscopy of Isolated Compounds

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The NMR spectra of the isolated compounds were recorded using an AV III 300 (300 MHz) and a DRX-600 (600 MHz) instrument (Bruker Daltonik, Billerica, MA, USA). The solvents used were chloroform-d₁ and acetone-d₆ from Eurisotop (Saint-Aubin, France). The spectra obtained were referenced using the residual signals (CDCl₃: δ (¹H) = 7.26 ppm and δ(¹³C) = 77.16 ppm; acetone-d₆: δ (¹H) = 2.05 ppm and δ(¹³C) = 29.84 ppm). MestreNova 14.2.1 purchased from Mestrelab Research S.L. (Santiago de Compostela, Spain) was used to process the spectra.

Sagurna L., Heinrich S., Kaufmann L.S., Rückert-Reed C., Busche T., Wolf A., Eickhoff J., Klebl B., Kalinowski J, & Bandow J.E. (2023). Characterization of the Antibacterial Activity of Quinone-Based Compounds Originating from the Alnumycin Biosynthetic Gene Cluster of a Streptomyces Isolate. Antibiotics, 12(7), 1116.

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Synthesis and Characterization of Fluorinated Polymers

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Vinylidene fluoride (VDF) and tert-butyl 2-(trifluoromethyl)acrylate (MAF-TBE) were kindly supplied by Arkema and Tosoh Finechem Corp., respectively, and used as received. Complexes 1, 2, 3, 5, and 6 were synthesized as described in a previous contribution [23 (link)]. Dimethyl carbonate (DMC, ≥99%, Merck KGaA), acetone (VMR Chemicals), pentane (VMR Chemicals), dimethyl formamide (VMR Chemicals), benzene-d₆ (99.5%D, Eurisotop), acetone-d₆ (99.5%D, Eurisotop), DMSO-d₆ (99.5%D, Eurisotop) and DMF-d₇ (99.5%D, Eurisotop) were used as received.

Morales-Cerrada R., Ladmiral V., Gayet F., Fliedel C., Poli R, & Améduri B. (2020). Fluoroalkyl Pentacarbonylmanganese(I) Complexes as Initiators for the Radical (co)Polymerization of Fluoromonomers. Polymers, 12(2), 384.

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Catechin hydrate extraction and analysis

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(+)-Catechin hydrate ≥ 98%; laccase from Trametes versicolor (0.94 U·mg⁻¹); sodium phosphate dibasic dihydrate ≥ 98%; citric acid (ACS reagent, cadmium nitrate tetrahydrate 99.997%; formic acid and Amberlite XAD7HP were obtained from Sigma-Aldrich) (Saint-Louis, MO, USA). Acetone-d₆ was purchased from Euriso-top (Saarbrücken, Germany), and trifluoroacetic acid (TFA) from Roth Labo (Karlsruhe, Germany). Water LC-MS, acetonitrile LC-MS (ACN), and methanol LC-MS (MeOH) were all from VWR (Radnor, PA, USA).

Deshaies S., le Guernevé C., Suc L., Mouls L., Garcia F, & Saucier C. (2021). Unambiguous NMR Structural Determination of (+)-Catechin—Laccase Dimeric Reaction Products as Potential Markers of Grape and Wine Oxidation. Molecules, 26(20), 6165.

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Lipase-Catalyzed Choline Chloride Synthesis

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Lipase B from Candida antarctica, immobilized on acrylic resin (former Novozyme 435) and choline chloride (98%) were purchased from Sigma-Aldrich (Sigma-Aldrich, St. Louis, USA). CDCl₃ (99.8%) and acetone-d6 (>99.9%) were from Eurisotop (Gif-sur-Yvette Cedex, France). Activated carbon was acquired from Carl Roth (Carl Roth KG, Karlsruhe, Germany). Fatty acids were purchased from Tokyo Chemical Industry Co. Ltd (TCI-Europe, Zwijndrecht, Belgium). All solvents were purchased in the highest purity available and used without further treatment.

Siebenhaller S., Hajek T., Muhle-Goll C., Himmelsbach M., Luy B., Kirschhöfer F., Brenner-Weiß G., Hahn T., Zibek S, & Syldatk C. (2017). Beechwood carbohydrates for enzymatic synthesis of sustainable glycolipids. Bioresources and Bioprocessing, 4(1), 25.

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Synthetic Methodology for Trifluoromethanesulfonamide

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Potassium hydroxide (KOH, Scharlab), acetone (99%, Scharlab), difluoromethanesulfonyl chloride (CF₂HSO₂Cl, Manchester Organics Limited), 1-methylimidazole (Sigma-Aldrich), acetonitrile (anhydrous, 99.9%, Thermo-Scientific), hydrochloric acid (HCl, 37%, Scharlab), tert-butyl methyl ether (MTBE, anhydrous, 99.8%, Sigma-Aldrich), potassium hydrogen carbonate (KHCO₃, Thermo-Scientific), and deuterated acetone (acetone-d₆, Eurisotop, 99.8% D) were used as purchased. Trifluoromethanesulfonamide (CF₃SO₂NH₂) was a generous gift from Solvay.

Sánchez-Diez E., Garcia L., Arcelus O., Qiao L., San Felices L., Carrasco J., Armand M., Martínez-Ibañez M, & Zhang H. (2023). Crystal structure and cation-anion interactions of potassium (Difluoromethanesulfonyl) (trifluorome thanesulfonyl)imide. Frontiers in Chemistry, 11, 1191394.

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