Copper nitrate trihydrate

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Copper nitrate trihydrate is a chemical compound with the formula Cu(NO3)2·3H2O. It is a blue, crystalline solid that is soluble in water and other polar solvents. The compound is commonly used in various industrial and laboratory applications.

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Copper (II) nitrate trihydrate (8 citations) Copper nitrate (6 citations)

6 protocols using copper nitrate trihydrate

Synthesis of Zeolite-Based Catalysts

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For this study, high-quality analytical reagents were obtained from reputable suppliers. Specifically, 30% hydrogen peroxide (H₂O₂), magnesium oxide (MgO), and potassium hydroxide (KOH) were sourced from Lach-Ner, s.r.o. (Neratovice, Czech Republic). Sodium silicate with a silicate modulus of 3.22 was provided by Labar s.r.o (Ústí nad Labem, Czech Republic). Zeolite ZEOCEM 50 (ZZ50) in powdered form with a particle size fraction of 560–850 μm was procured from Zeocem (Bystré, Slovakia). Additionally, metal nitrates, including copper nitrate trihydrate (Cu(NO₃)₂·3H₂O) and nickel(II) nitrate hexahydrate (Ni(NO₃)₂·6H₂O), were obtained from Acros Organics B.V.B.A., (Geel, Belgium) and Penta, s.r.o., (Prague, Czech Republic), respectively, to facilitate the experimental procedures.

Svobodová E., Tišler Z., Peroutková K., Strejcová K., Abrham J., Šimek J., Gholami Z, & Vakili M. (2024). Adsorption of Cu(II) and Ni(II) from Aqueous Solutions Using Synthesized Alkali-Activated Foamed Zeolite Adsorbent: Isotherm, Kinetic, and Regeneration Study. Molecules, 29(10), 2357.

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Synthesis of Metal-Organic Frameworks

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All chemicals used in this work are commercially available: copper nitrate trihydrate (99%, Acros Organics), magnesium nitrate hexahydrate (99%, Sigma-Aldrich), 1,3,5-tricarboxybenzene (95%, Strem Chemicals), ethanol (91%, Pharmco). These chemicals were directly utilized in all experiments without any further purification. Deionized water from the Milli-Q water purification system was used in all experiments.

Liu Y., Liu S., Gonçalves A.A, & Jaroniec M. (2018). Effect of metal–ligand ratio on the CO2 adsorption properties of Cu–BTC metal–organic frameworks. RSC Advances, 8(62), 35551-35556.

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Synthesis and Characterization of Inorganic Compounds

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l-Histidine hydrochloride monohydrate was purchased from TCI (Tokyo, Japan). Potassium nitrate (>99.0%), silver nitrate (>99.0%), and sodium chloride (>99.0%) were purchased from Sigma-Aldrich (St. Louis, MO, USA). Copper nitrate trihydrate (>99.0%), lead nitrate (>99.0%), and sodium bromide (99.5%) were purchased from Acros (Morris Plains, NJ, USA). Magnesium nitrate hexahydrate (>98.0%) and sodium iodide (>99.0%) were procured from SHOWA (Tokyo, Japan). Cobalt chloride (97.0%), iron chloride (98.0%), and mercury chloride (>98.0%) were obtained from Alfa Aesar (Heysham, England). Calcium nitrate tetrahydrate (>99.0%) and manganese chloride dehydrate (>99.0%) were purchased from Merck (Kenilworth, NJ, USA). Monobasic, dibasic, and tribasic sodium salts of phosphate, phosphoric acid (85.0%), sodium hydroxide (98.0%), and zinc nitrate hexahydrate (>99.0%) were obtained from J.T. Baker (Center Valley, PA, USA). Ultrapure water (18.2 MΩ cm) from a Milli-Q system (Millipore, Billerica, MA, USA) was used to prepare all solutions.

Lin Y.S., Lin Y., Periasamy A.P., Cang J, & Chang H.T. (2019). Parameters affecting the synthesis of carbon dots for quantitation of copper ions. Nanoscale Advances, 1(7), 2553-2561.

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Synthesis and Catalytic Evaluation of Cu(BTC) MOF

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All reagents were commercially available and used without further purification. For the synthesis of the Cu(BTC) MOF, we used copper nitrate trihydrate (Cu(NO 3 ) 2 •3H 2 O, 99%) provided by Acros Organics and trimesic acid (benzene-1,3,5-tricarboxylic acid, C 9 H 6 O 6 , 95%) supplied by Sigma-Aldrich. Part of the nitrophenols employed in the catalytic tests, more specifically, 2-nitrophenol (C 6 H 5 NO 3 , 99%) and 4-nitrophenol (C 6 H 5 NO 3 , 99%), were purchased from Thermo Scientific, while the rest of the reagents used for the catalytic evaluation such as sodium borohydride (NaBH 4 , 96%), 4-nitrobenzoic acid (C 7 H 5 NO 4 , 98%) and 4-nitrobenzamide (C 7 H 6 N 2 O 3 , 98%) were purchased from Sigma-Aldrich.

Chamorro-Mena I., Linares N, & García-Martínez J. (2023). Blue-LED activated photocatalytic hydrogenation of nitroarenes with Cu₂O/CuO heterojunctions. Dalton transactions (Cambridge, England : 2003), 52(37).

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Synthesis of Metal-Organic Frameworks

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Zinc nitrate hexahydrate (99%, CAS# 10196-18-6), copper nitrate trihydrate (99%, CAS# 10031-43-3), cobalt nitrate hexahydrate (99% CAS# 10026-22-9), 2-methylimidazole (99%, CAS# 693-98-1), boric acid (≥99.5%, CAS# 10043-35-3), ethanol (≥99.8%, CAS# 64-17-5), and melamine (99%, CAS# 108-78-1) were purchased from Fisher Scientific. All chemicals were used as received. The gases used in this study, NH₃ (99.98%), N₂ (99.9995%), and CO₂ (99.999%) were purchased from BOC. H₂ (99.9995%) was generated locally from deionized water using a Peak Scientific PH200 hydrogen generator.

Tian T., Xu J., Xiong Y., Ramanan N., Ryan M., Xie F, & Petit C. (2022). Cu-functionalised porous boron nitride derived from a metal–organic framework. Journal of Materials Chemistry. a, 10(38), 20580-20592.

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Synthesis of Substituted Benzene Dicarboxylates

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Materials and reagents were obtained from multiple
different commercial
suppliers and used without further purification, specifically: dimethoxy-2,5-dihydroxybenzenedicarboxylate
(Sigma-Aldrich, 99+%), methyl iodide (Alfa Aesar, 99%, stabilized
with copper), ethyl bromide (Sigma-Aldrich, 98%), propyl bromide (Sigma-Aldrich,
99%), butyl bromide (Acros, 99%), pentyl bromide (Alfa Aesar, 99%),
copper nitrate trihydrate (SLS, 98%), acetonitrile (Fisher, ≥
99.9%) and n,n-dimethylformamide
(Fisher, ≥99%).

Ashworth D.J., Roseveare T.M., Schneemann A., Flint M., Dominguez Bernáldes I., Vervoorts P., Fischer R.A., Brammer L, & Foster J.A. (2019). Increasing Alkyl Chain Length in a Series of Layered Metal–Organic Frameworks Aids Ultrasonic Exfoliation to Form Nanosheets. Inorganic Chemistry, 58(16), 10837-10845.

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