The activated coal (SX+) was obtained from NORIT. The reduced graphene oxide N002-PDR (RGO) was obtained from Angstron Materials. The carbon multi-walled nanotubes (MWCNT) were obtained from Nanocyl (Belgium) (NC 7000 Thin MWCNTs, 95+% C purity). The carbon black (CB) was obtained as 250 G type from IMERYS GRAPHITE & CARBON. The carbon nanofibers (CNF; LHT type) were obtained from Applied Sciences Inc (USA). The graphene nanoplatelets (GNP; M15, and C750 types) were purchased from Sigma-Aldrich. Sulfanilic acid (99%), isopentyl nitrite (96%), D-(+)-cellobiose (≥99%), cellulose (reference C6288, crystalline and high purity) were also supplied by Sigma-Aldrich and used as received.
Isopentyl nitrite
Manufactured by Merck Group
Sourced in United States
Isopentyl nitrite is a colorless, volatile liquid organic compound. Its core function is as a chemical reagent used in organic synthesis, particularly in the preparation of various nitro compounds and other nitrite esters.
Automatically generated - may contain errors
Lab products found in correlation
Sulfanilic acid, by Merck Group (2 mentions)
D cellobiose, by Merck Group (1 mentions)
Acetonitrile, by Chempur (1 mentions)
Methyl ethyl ketone, by Merck Group (1 mentions)
Acetic acid, by Chempur (1 mentions)
Sulfuric acid, by Chempur (1 mentions)
Cyclopentanone, by Merck Group (1 mentions)
Methanol, by Chempur (1 mentions)
Cyclohexanone, by Merck Group (1 mentions)
Manganese 2 acetylacetonate, by Merck Group (1 mentions)
Cobalt 2 acetate tetrahydrate, by Merck Group (1 mentions)
Manganese 2 acetate tetrahydrate, by Merck Group (1 mentions)
Cobalt 2 acetylacetonate, by Merck Group (1 mentions)
Tert butyl nitrite, by Merck Group (1 mentions)
Cobalt 2 nitrate hexahydrate, by Merck Group (1 mentions)
Cyclohexane, by Merck Group (1 mentions)
Nitric acid, by Merck Group (1 mentions)
Benzonitrile, by Merck Group (1 mentions)
Cyclohexanol, by Merck Group (1 mentions)
1 2 dichlorobenzene, by Merck Group (1 mentions)
5 protocols using isopentyl nitrite
1
Synthesis of Functionalized Carbon Nanomaterials
2
Graphene-Based Cementitious Composites
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The commercial pristine GBM employed in the present study are listed below along with their main features, as declared in the technical data sheets.
- GBM 1: FLG powder (1–5 layers), with an average lateral size of up to 9 μm, and 99.9% C; supplied by Proton Power.
- GBM 2: SLG powder, with an average lateral size of up to 5 μm, and 99.9% C; purchased from Carlo Erba.
- GBM 3: FLG powder (6–10 layers), with an average lateral size of up to 1 μm, and more than 95% C; supplied by NanoXplore.
- GBM 4: FLG powder (6–10 layers), with an average lateral size of up to 2 μm, and more than 91% C; supplied by NanoXplore.
The cement used was a white Roccabianca 42.5R Portland cement, type CEM II/B-LL 42.5 R, that was supplied by Italcementi S.p.A., while the Creactive-IVK superplasticizer (SP), a specific admixture for mortars based on polycarboxylate ether polymers, was produced by Sika Italia S.p.A. Aniline-4-sulfonic acid and isopentyl nitrite were purchased from Sigma Aldrich and used as received.
- GBM 1: FLG powder (1–5 layers), with an average lateral size of up to 9 μm, and 99.9% C; supplied by Proton Power.
- GBM 2: SLG powder, with an average lateral size of up to 5 μm, and 99.9% C; purchased from Carlo Erba.
- GBM 3: FLG powder (6–10 layers), with an average lateral size of up to 1 μm, and more than 95% C; supplied by NanoXplore.
- GBM 4: FLG powder (6–10 layers), with an average lateral size of up to 2 μm, and more than 91% C; supplied by NanoXplore.
The cement used was a white Roccabianca 42.5R Portland cement, type CEM II/B-LL 42.5 R, that was supplied by Italcementi S.p.A., while the Creactive-IVK superplasticizer (SP), a specific admixture for mortars based on polycarboxylate ether polymers, was produced by Sika Italia S.p.A. Aniline-4-sulfonic acid and isopentyl nitrite were purchased from Sigma Aldrich and used as received.
3
Oxidative Functionalization of Cyclic Ketones
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The following were used: cyclopentanone (Sigma-Aldrich, St. Louis, MI, USA, ≥99%), cyclohexanone (Sigma-Aldrich, ≥99%), cycloheptanone (Sigma-Aldrich, ≥99%), cyclooctanone (Sigma-Aldrich, ≥98%), cyclododecanone (Merck, Rahway, NJ USA, ≥98%), 2-methylcyclohexanone (Aldrich, St. Louis, MI, USA, ≥98%), 3-methylcyclohexanone (Aldrich, ≥97%), 4-methylcyclohexanone (Aldrich, ≥99%), cyclohexanol (Sigma-Aldrich, >99%), cyclohexane (Sigma-Aldrich, >99%), manganese(II) acetylacetonate (Sigma-Aldrich, 99%), cobalt(II) acetylacetonate (Sigma-Aldrich, 97%), manganese(II) acetate tetrahydrate (Sigma-Aldrich, 99.99%), cobalt(II) acetate tetrahydrate (Sigma-Aldrich, 99.99%), manganase(II) nitrate tetrahydrate (Sigma-Aldrich, ≥97%), cobalt(II) nitrate hexahydrate (Sigma-Aldrich, >99%), isopentyl nitrite (Sigma-Aldrich, 96%), tert-butyl nitrite (Sigma-Aldrich, 90%), N-hydroxyphthalimide (Acros, Waltham, MA, USA, 98%), methyl ethyl ketone (Sigma-Aldrich, 99.7%), nitric acid (Sigma-Aldrich, 60%), pentyl nitrite (Sigma-Aldrich, 98%), acetic acid (Chempur, Karlsruhe, Germany, 99.5%), acetonitrile (Chempur, 99.5%), benzonitrile (Sigma-Aldrich, 99%), sulfuric acid (Chempur, 98%), and methanol (Chempur, 99.8%).
4
Synthesis of Molybdenum Disulfide Composites
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All organic solvents were
high-performance liquid chromatography (HPLC)-grade and used without
further purification. Bulk molybdenum disulfide powder (from ∼6
μm to a maximum of 40 μm, 98%, product number 69860, batch
number WXBD2352V) was purchased from Sigma-Aldrich and used without
further purification. Iron(II) chloride tetrahydrate, cobalt(II) chloride,
zinc(II) chloride, and copper(II) chloride were purchased from Sigma-Aldrich.
4-nitrobenzenediazonium tetrafluoroborate (97%), sodium tetrafluoroborate
(98%), sodium nitrite (reagent plus, ≥99%), nitrobenzene (≥99%),
1,2-dichlorobenzene (anhydrous, 99%), isopentyl nitrite (96%), acetonitrile
(HPLC gradient grade, ≥99.9%), N,N-dimethylformamide (≥99.8%), diethyl ether (HPLC, ≥99.9%,
inhibitor-free), Whatman poly(tetrafluoroethylene) (PTFE) membrane
filters (PTFE membrane circles, TE 36, 0.45 μm, 47 mm), and
4-tert-butylaniline (99%) were purchased from Sigma-Aldrich.
Water used for experiments was ultrapure type I water (18.2 MΩ
cm) from a Millipore Simplicity water purification system.
high-performance liquid chromatography (HPLC)-grade and used without
further purification. Bulk molybdenum disulfide powder (from ∼6
μm to a maximum of 40 μm, 98%, product number 69860, batch
number WXBD2352V) was purchased from Sigma-Aldrich and used without
further purification. Iron(II) chloride tetrahydrate, cobalt(II) chloride,
zinc(II) chloride, and copper(II) chloride were purchased from Sigma-Aldrich.
4-nitrobenzenediazonium tetrafluoroborate (97%), sodium tetrafluoroborate
(98%), sodium nitrite (reagent plus, ≥99%), nitrobenzene (≥99%),
1,2-dichlorobenzene (anhydrous, 99%), isopentyl nitrite (96%), acetonitrile
(HPLC gradient grade, ≥99.9%), N,N-dimethylformamide (≥99.8%), diethyl ether (HPLC, ≥99.9%,
inhibitor-free), Whatman poly(tetrafluoroethylene) (PTFE) membrane
filters (PTFE membrane circles, TE 36, 0.45 μm, 47 mm), and
4-tert-butylaniline (99%) were purchased from Sigma-Aldrich.
Water used for experiments was ultrapure type I water (18.2 MΩ
cm) from a Millipore Simplicity water purification system.
5
Graphene-Based Nanocomposite Synthesis
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Reagents were used as purchased from commercial sources without further purification. SP-1 graphite powder was purchased from Bay Carbon, Inc. and glycine was from Acros Organics (98%). Isopentyl nitrite, sulfanilic acid, acrylamide (AM) and N,N′-methylenebisacrylamide (MBA) were purchased from Sigma Aldrich. IRGACURE 2959 was purchased from TCI Chemicals. Dichloromethane was purchased from Scharlab and ethanol was from Labkem. A planetary ball mill (Retsch PM 100) was used to prepare FLG. Milli-Q water was generated using a Simplicity® UV Water Purification System. SH-SY5Y cells were purchased from ATCC. Culture media, plates, fluorophores, antibodies and reagents used for cell viability and immunochemistry experiments were purchased from Thermo Fisher (MA, USA). All-trans retinoic acid (ATRA) was purchased from Sigma-Aldrich and brain-derived neurotrophic factor (BDNF) was purchased from Thermo Fisher Scientific.
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