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Allylamine

Manufactured by Thermo Fisher Scientific
Sourced in United Kingdom, Germany, India

Allylamine is a chemical compound used in various laboratory applications. It serves as a building block for the synthesis of other organic compounds. Allylamine is a colorless liquid with a distinctive, amine-like odor. It is soluble in common organic solvents. The specific applications and use of allylamine may vary depending on the needs of the laboratory.

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3 protocols using allylamine

1

Synthesis and Characterization of Allylamine-Choline Composite

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Allylamine (C3H7N, 98%) and choline chloride were [(CH3)3NCH2CH2OH]+Cl purchased from Alfa Aesar (Heysham, England). D-glucose (C6H12O6, 99.5%), methylene blue (C16H18N3ClS, 95%), and methyl orange (C14H14N3NaO3S, 85%), methanol (CH3OH, 99.9%) were purchased from Sigma-Aldrich (Burghausen, Germany). All chemicals used in this study were of analytical grade and used without further purification. All the solutions were made with high-purity water with 18 MΩ×cm resistance.
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2

Synthesis of Hexachlorocyclotriphosphazene Derivatives

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Hexachlorocyclotriphosphazene (98%) was purchased from Acros organics; 3-mercaptopropionic acid (99%) and allylamine (>98%) from Alfa Aesar (Karlsruhe, Germany); 2,2-dimethoxy-2-phenylacetophenone (DMPA) (99%) and (3-mercaptopropyl)trimethoxysilane (95%) were obtained from Sigma-Aldrich (Vienna, Austria); anhydrous THF, trimethylamine and cetyltrimethylammonium bromide (CTAB) (≥99%) from VWR (Vienna, Austria); ethanol (99%) from Fluorochem (Derbyshire, UK); and NaOH (98%) from J. T. Baker (Fisher Scientific, Wien, Austria). Deuterated chloroform and methanol for NMR experiments from Eurisotop (Saint Aubin, France). Triethylamine was distilled before usage for the substitution reaction. All other chemicals and solvents were used as received.
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3

Synthesis of Copper(II) Complexes and Derivatives

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The chemicals used were obtained from the following sources: Trifluroacetic acid from SRL; sodium acetate from SD Fine-chem; sodium benzoate, copper hydroxide carbonate, triethylamine from Merck, India and allyl amine from Alfa Aesar. Copper(II) perchlorate hexa-hydrate was freshly prepared by treating hydrated copper(II) carbonate (22.12 g, 0.1 mol) with 1:1 aqueous solution of perchloric acid. Sodium trifluroacetate was prepared by treating sodium hydroxide (4.00 g, 0.1 mol) and trifluroacetic acid (11.40 g, 0.1 mol) in water. 2,6-diformyl-4-methylphenol (2-hydroxy-5-methyl-benzene-1,3-dicarbaldehyde) was prepared following a modified literature procedure providing a better yield. 16 All the chemicals and solvents used in this work were of reagent grade and used as received without further purification.
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