ICP-OES was performed using an iCAP 6300 Duo ICP-OES spectrometer (Thermo Scientific). Prior to measurements, the samples were weighed and fully dissolved in HNO3.
Icap 6300 duo icp oes spectrometer
Manufactured by Thermo Fisher Scientific
Sourced in United States
The ICAP 6300 DUO ICP-OES spectrometer is an inductively coupled plasma optical emission spectrometer designed for elemental analysis. It utilizes a dual configuration with two optical paths to provide simultaneous measurement of elements at multiple wavelengths.
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8 protocols using icap 6300 duo icp oes spectrometer
1
Elemental Analysis by ICP-OES
2
Quantifying Metal Ratios with ICP-OES and SEM-EDX
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Inductively coupled plasma optical
emission spectroscopy (ICP-OES) was performed with an iCAP 6300 DUO
ICP-OES spectrometer (ThermoScientific) to quantify the Cu/Zn and
Mn/Zn ratios with a systematic error of about 5%. Samples for ICP-OES
measurements were dissolved in 1 mL of aqua regia (HCl/HNO3 = 3/1(v/v)) overnight. Scanning electron microscopy (SEM) was performed
on a HRSEM JEOL JSM-7500LA microscope with a cold field-emission gun
(FEG), operating at 15 kV acceleration voltage. To evaluate the full
elemental composition of these samples, energy-dispersive spectroscopy
(EDX, Oxford instrument, X-Max, 80 mm2) was operated at
8 mm working distance, 15 kV acceleration voltage, and 15 sweep count.
emission spectroscopy (ICP-OES) was performed with an iCAP 6300 DUO
ICP-OES spectrometer (ThermoScientific) to quantify the Cu/Zn and
Mn/Zn ratios with a systematic error of about 5%. Samples for ICP-OES
measurements were dissolved in 1 mL of aqua regia (HCl/HNO3 = 3/1(v/v)) overnight. Scanning electron microscopy (SEM) was performed
on a HRSEM JEOL JSM-7500LA microscope with a cold field-emission gun
(FEG), operating at 15 kV acceleration voltage. To evaluate the full
elemental composition of these samples, energy-dispersive spectroscopy
(EDX, Oxford instrument, X-Max, 80 mm2) was operated at
8 mm working distance, 15 kV acceleration voltage, and 15 sweep count.
3
ICP-OES Analysis of Nanoparticles
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ICP elemental analysis was performed by inductively coupled plasma optical emission spectroscopy (ICP-OES) using a ThermoScientific (Waltham, MA, USA) iCAP 6300 DUO ICP-OES spectrometer. Chemical analyses by ICP-OES are affected by a systematic error of 5%. Furthermore, 30–50 µL of a BGNP sample was dissolved overnight in 1 mL of aqua regia and then diluted to 10 mL with ultraclean deionized water before analysis.
4
ICP-OES Analysis of Elemental Composition
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ICP elemental analysis was carried out via inductively
coupled plasma
optical emission spectroscopy (ICP-OES) with an iCAP 6300 DUO ICP-OES
spectrometer (ThermoScientific). All chemical analyses performed by
ICP-OES were affected by a systematic error of about 5%. The samples
were dissolved in nitric acid (HNO3 68% (v/v)) and heated
to 180 °C for 45 min in a microwave reactor (CEM MARS5). After
this step, Cs+, Mn2+, and In3+ ions
were dissolved in the acid solution, while AgCl precipitated, due
to its very low solubility. The AgCl white solid was thus separated
from the acid solution via centrifugation. The supernatant was diluted
using Milli-Q water and analyzed, without any further operations,
to determine the concentration of Mn2+ and In3+ ions. It is worth noting here that no traces of Ag+ ions
were detected in this solution. The AgCl precipitate, on the other
hand, was reacted with ammonia (0.5 mL of NH3 solution
in water) to form water-soluble complexes,55 which were diluted with Milli-Q water and analyzed.
coupled plasma
optical emission spectroscopy (ICP-OES) with an iCAP 6300 DUO ICP-OES
spectrometer (ThermoScientific). All chemical analyses performed by
ICP-OES were affected by a systematic error of about 5%. The samples
were dissolved in nitric acid (HNO3 68% (v/v)) and heated
to 180 °C for 45 min in a microwave reactor (CEM MARS5). After
this step, Cs+, Mn2+, and In3+ ions
were dissolved in the acid solution, while AgCl precipitated, due
to its very low solubility. The AgCl white solid was thus separated
from the acid solution via centrifugation. The supernatant was diluted
using Milli-Q water and analyzed, without any further operations,
to determine the concentration of Mn2+ and In3+ ions. It is worth noting here that no traces of Ag+ ions
were detected in this solution. The AgCl precipitate, on the other
hand, was reacted with ammonia (0.5 mL of NH3 solution
in water) to form water-soluble complexes,55 which were diluted with Milli-Q water and analyzed.
5
Elemental Analysis via ICP-OES
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The elemental analysis
was also performed via inductively coupled plasma optical emission
spectroscopy (ICP-OES) with an iCAP 6300 DUO ICP-OES spectrometer
(ThermoScientific). The samples were dissolved in 1 mL of aqua regia
(HCl/HNO3 = 3/1 (v/v)) overnight and then diluted with
9 mL of Milli-Q water for measurements. The elemental analysis using
ICP-OES was affected by a systematic error of ∼5%.
was also performed via inductively coupled plasma optical emission
spectroscopy (ICP-OES) with an iCAP 6300 DUO ICP-OES spectrometer
(ThermoScientific). The samples were dissolved in 1 mL of aqua regia
(HCl/HNO3 = 3/1 (v/v)) overnight and then diluted with
9 mL of Milli-Q water for measurements. The elemental analysis using
ICP-OES was affected by a systematic error of ∼5%.
6
Elemental Analysis of Mg Calcite
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ICP‐OES was performed using an iCAP 6300 Duo ICP‐OES spectrometer (Thermo Scientific) for elemental analysis. Samples were weighed before analysis, immersed in 0.6 m HCl, and placed on a rocking table for 24 h to dissolve the Mg calcite.[27 ] Later, insoluble organics were separated from the solution and their weight was subtracted for accurate analysis.
7
Quantification of Cu-Zn Ratio by ICP-OES
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ICP elemental analysis performed
via inductively coupled plasma optical
emission spectroscopy (ICP-OES) with an iCAP 6300 DUO ICP-OES spectrometer
(ThermoScientific) was used to quantify the Cu-to-Zn ratio. All chemical
analyses performed by ICP-OES were affected by a systematic error
of about 5%. The samples were dissolved with 1 mL of aqua regia (HCl/HNO3 = 3/1(v/v)) overnight.
via inductively coupled plasma optical
emission spectroscopy (ICP-OES) with an iCAP 6300 DUO ICP-OES spectrometer
(ThermoScientific) was used to quantify the Cu-to-Zn ratio. All chemical
analyses performed by ICP-OES were affected by a systematic error
of about 5%. The samples were dissolved with 1 mL of aqua regia (HCl/HNO3 = 3/1(v/v)) overnight.
8
ICP-OES Elemental Analysis Protocol
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The ICP elemental analysis was carried out via inductively coupled plasma optical emission spectroscopy (ICP-OES) using an iCAP 6300 DUO ICP-OES spectrometer (Thermo Scientific) operating at an RF power of 1150 W, using a flush pump rate of 100 rpm, an auxiliary gas flow rate of 0.5 l min–1 and an analysis pump rate of 45 rpm. The samples were dissolved overnight in HCl/HNO3 at 3 : 1 (v/v) and diluted with Milli-Q before analysis.
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