Analyses were performed using a Thermo Nicolet 8700 FTIR Spectrometer and Continuum FTIR Microscope. Samples were prepared by drop coating a toluene dispersion of the solid sample in question onto an electronics-grade Si-wafer (N-type, 100 surface, 100 mm thickness and 10 ohm cm resistivity) and dried under flowing nitrogen.
Ft ir microscope
Manufactured by Thermo Fisher Scientific
Sourced in United States
The FT-IR microscope is a laboratory instrument designed for the analysis of small samples. It combines the capabilities of a Fourier Transform Infrared Spectrometer (FT-IR) with a microscope, allowing for the identification and characterization of materials at the microscopic level.
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3 protocols using ft ir microscope
1
FTIR Analysis of Solid Samples
2
FT-IR Analysis of RPDF Variants
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The FT-IR spectral characteristics of RPDF, HT-RPDF, and FT-RPDF were analyzed using an FT-IR microscope (Thermo Fisher Scientific, Waltham, MA, USA). Briefly, 3 mg of each sample was thoroughly mixed with 150 mg of KBr power in an agate mortar, ground, and then pressed into about 1 mm thick pellets. The resulting pellets were scanned in the range of 400–4000 cm−1 using Nicolet IS50-Nicolet Continuum (Thermo Scientific, Waltham, MA, USA).
3
FT-IR Spectroscopy of Samples
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FT-IR microscope (Thermo Scientific Inc., USA) with liquid nitrogen cooled MCT-A detector has been used, conical shape germanium tip crystal (350-micron spherical finish, single reflection, throughput > 50%, 27° average angle). Each spectrum has been achieved in the range of 4000–650 cm−1 at a spectral resolution of 8 cm−1 and with 128 scans on the average using Omnic software (Thermo Sci- entific Inc., USA).
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