All chemicals and solvents were purchased from Sigma-Aldrich and Merck chemical companies and were used without extra purification. The surface morphology and diameter of the CoFe2O4/AA-M (Co, V) nanocatalysts were studied by scanning electron microscopy (FE-SEM) analysis data was recorded SEM-TESCAN MIRA3. Transmission electron microscopy (TEM) was carry out using a FEI CM200 field emission at accelerating voltage of 80 kV. The XRD was recorded on JEOL JSM-6100 microscope with (Cu Kα radiation, λ = 1.54 Å). The thermal gravimetric analysis (TGA) of nanocomposite was carried out on a Shimadzu analyzer DTG-60. Magnetic properties of the samples were determined using a vibrating sample magnetometer (VSM) at room temperature (MDKFD, University of Kashan, Iran). The amounts of Co and V in synthesized the nanocatalysts were evaluated by plasma-optical emission spectrometry (ICP-OES). Infrared (FT-IR) spectra of all samples were recorded on PerkinElmer Spectrum one instruments, using KBr pellets in the range of 400–4000 cm−1.
Jsm 6100 microscope
Manufactured by JEOL
The JSM-6100 is a scanning electron microscope (SEM) manufactured by JEOL. It is designed for high-resolution imaging and analysis of a wide range of materials. The JSM-6100 utilizes an electron beam to scan the surface of a sample, generating detailed images with high magnification and depth of field. The microscope is capable of producing images with a resolution up to 3.0 nanometers, making it suitable for a variety of applications in materials science, biology, and other fields.
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Lab products found in correlation
2 protocols using jsm 6100 microscope
1
Characterization of CoFe2O4/AA-M (Co, V) Nanocatalysts
2
Comprehensive Material Characterization
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The Bruker D8 Advance instrument was used for X-ray diffraction (XRD) study. The Jeol JEM-1010 electron microscope with iTEM software was used for the TEM study. High-resolution TEM images were recorded with Jeol JEM 2100 Electron Microscope. A JEOL JSM-6100 microscope was used for both SEM and EDX studies. The DeltaNu advantage 532™ Raman instrument was used for Raman spectra.
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