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2 protocols using sodium n hexadecyl sulfate

1

Evaluation of Surfactants and Phospholipids

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Bis(2-ethylhexyl) phosphate,
dibenzyl phosphate, mono-n-dodecyl phosphate, n-octanol, sodium 1-dodecane sulfonate, sodium n-hexadecyl sulfate, sodium n-octyl sulfate, sodium
1-pentyl sulfate, and taurocholic acid sodium salt hydrate were purchased
from Alfa Aesar (Germany). Sodium 1-octanesulfonic acid sodium salt
monohydrate (sodium 1-octane sulfonate) was received from MP Biomedicals
(France). 6, 9-Diamino-2-ethoxyacridine-dl-lactate monohydrate
(ethacridine lactate salt), dihexadecyl phosphate, 1,2-dioleoyl-sn-glycero-3-phosphate
sodium salt (DOPA), 4-(2-hydroxyethyl)piperazine-1-ethanesulfonic
acid (HEPES), hexadecyl phosphonic acid, oleyl alcohol, potassium
cetyl phosphate, sodium 1-butanesulfonate suitable for ion pair chromatography,
sodium docusate (purum), sodium dodecylbenzene sulfonate, sodium 1-heptane
sulfonate, sodium hexane sulfonate, and Tween 80 (polyoxyethylene
(20) sorbitan monooleate) were obtained from Sigma Aldrich (Austria).
Kolliphor EL (Cremophor EL) and medium chain triglycerides (Labrafac
lipophile WL 1349) were kind gifts from BASF (Germany) and Gattefossé
(France), respectively. SpectraPor Float-A-Lyzer G2 Dialysis Devices
(MWCO 3.5–5 kD) were purchased from Lactan (Austria).
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2

Synthesis and Characterization of Amphiphilic Compounds

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AmB (>95 % purity) was purchased from Cayman Chemical Co. (Ann Arbor, MI). Hydroxypropylmethyl Acetate Succinate 912 (HPMCAS 912) was donated by The Dow Chemical Company (Midland, MI). Polyvinylpyrrolidone K30 (PVP K30) was donated from BASF (Ludwigshafen, Germany). Sodium dodecyl sulfate (12S) was obtained from BASF (Ludwigshafen, Germany). Sodium n-decyl sulfate (10S), sodium n-octyl sulfate (8S), and sodium n-hexadecyl sulfate (16S) were all purchased from Alfa Aesar (Ward Hill, MA). Sodium n-tetradecyl sulfate (14S) and sodium n-octadecyl sulfate (18S) were both purchased from Acros Organics B.V.B.A (Fair Lawn, NJ). Sodium decanoate (C10) and sodium dodecanoate (C12) were both obtained from Tokyo Chemical Industry (Tokyo, Japan). Dimethyl sulfoxide (DMSO), ethanol (EtOH), acetone, tetrahydrofuran (THF), and HPLC grade acetonitrile (ACN) and methanol (MeOH) were obtained from Sigma-Aldrich (St. Louis, MO).
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