Hardwood bleached kraft pulp (HwBKP) for CNF preparation was supplied by Moorim P&P (Ulsan, Korea). For the carboxymethylation process, monochloroacetic acid (Sigma Aldrich, St. Louis, MO, USA), sodium hydroxide, and isopropanol (Samchun Chemicals Co. Ltd., Seoul, Korea) were used. Epoxy resin (KDS 8128, Kukdo Chemical, Seoul, Korea) and a hardener (MH 700G, New Japan Chemical Co. Ltd., Osaka, Japan) were used for the preparation of the composite. 2,4,6-Tris(dimethylaminomethyl)phenol (Sigma Aldrich) was used as a catalyst for epoxy hardening.
2 4 6 tris dimethylaminomethyl phenol
Manufactured by Merck Group
Sourced in United States
2,4,6-tris(dimethylaminomethyl)phenol is a chemical compound used as a lab equipment product. It serves as a cross-linking agent and curing agent for epoxy resins.
Automatically generated - may contain errors
3 protocols using 2 4 6 tris dimethylaminomethyl phenol
1
Carboxymethylated Hardwood Pulp for CNF
2
Synthesis of Epoxy Polymer Composites
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3-Mercaptopropionic acid (3-MPA), trimethylolpropane (TMP), p-toluenesulfonic acid (p-TSA), and 2,4,6-tris(dimethylaminomethyl)phenol were purchased from Sigma-Aldrich (Milwaukee, WI, USA) and were used without further purification. The diglycidyl ether of bisphenol A (DGEBA) epoxy resin (EEW = 185 g eq−1) was supplied by Shin-A T&C (Seoul, Korea). Other organic solvents and chemicals were purchased from SAMCHUN Chemicals (Seoul, Korea).
3
Thermoset Polymer Synthesis and Characterization
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The starting materials (crotonic acid, thiourea,
1,4-butanediol, trimethylolpropane, and pentaerythritol) and the curing
base catalyst [2,4,6-tris(dimethylaminomethyl)phenol]
were purchased from Sigma-Aldrich (Milwaukee, WI, USA). p-Toluenesulfonic acid monohydrate (p-TSA) was purchased
from TCI Co., Ltd. (Tokyo, Japan). Other organic solvents and chemicals
were purchased from Daejung Chemical (Goryeong-gun, Korea). Epoxy
resin based on diglycidylether bisphenol-A (DGEBA; YD-128) with an
epoxy equivalent weight of 184–190 g/eq was donated from Kukdo
Chemical Co., Ltd. (Seoul, Korea).
1,4-butanediol, trimethylolpropane, and pentaerythritol) and the curing
base catalyst [2,4,6-tris(dimethylaminomethyl)phenol]
were purchased from Sigma-Aldrich (Milwaukee, WI, USA). p-Toluenesulfonic acid monohydrate (p-TSA) was purchased
from TCI Co., Ltd. (Tokyo, Japan). Other organic solvents and chemicals
were purchased from Daejung Chemical (Goryeong-gun, Korea). Epoxy
resin based on diglycidylether bisphenol-A (DGEBA; YD-128) with an
epoxy equivalent weight of 184–190 g/eq was donated from Kukdo
Chemical Co., Ltd. (Seoul, Korea).
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