Ta 60ws software

Manufactured by Shimadzu

Sourced in Japan

The TA-60WS software is a thermal analysis software developed by Shimadzu. It provides data analysis and control functions for thermal analysis instruments.

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Lab products found in correlation

Dsc 60, by Shimadzu (6 mentions) Dsc 60 instrument, by Shimadzu (1 mentions) S201 53090, by Shimadzu (1 mentions) Beadblaster 24, by Benchmark Scientific (1 mentions)

Spelling variants of this product

TA-60WS (27 citations) TA-60WS (2.20) software (2 citations)

11 protocols using ta 60ws software

Thermal Analysis of AMX and Excipients

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The DTA curves of AMX, binary mixtures, and pharmaceutical excipients were obtained on a simultaneous DTA/TGA DTG-60 (Shimadzu, Kyoto, Japan) thermal analyzer using an aluminum sample holder containing a 2 ± 0.1 mg sample under an atmosphere of nitrogen with a flow of 50 mL·min⁻¹. The samples were subjected to heating in a temperature range of 25 to 400 °C in programming of 10 °C·min⁻¹. For calibration of the equipment, Indium (melting point 156.6 °C) was used as the standard.
Thermogravimetry (TG) was only used for the characterization of the extract. Thus, the thermogravimetric curve of the AMX was obtained from a simultaneous thermal analyzer previously mentioned for DTA analysis, using an alumina sample holder containing 8.0 ± 0.5 mg of sample, under nitrogen atmosphere at a flow rate of 50.0 mL·min⁻¹ as the purge gas. The sample was conditioned at a temperature range of 25–900 °C at a heating rate of 10 °C·min⁻¹. The data were analyzed using the TA60-WS software (Shimadzu, Kyoto, Japan).

Almeida L., Júnior J.A., Silva M., Nóbrega F., Andrade J., Santos W., Ribeiro A., Conceição M., Veras G, & Medeiros A.C. (2019). Tablet of Ximenia Americana L. Developed from Mucoadhesive Polymers for Future Use in Oral Treatment of Fungal Infections. Polymers, 11(2), 379.

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Thermal Analysis of Organic Compounds

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DSC measurements were carried out using a Shimadzu DSC-60 instrument (Shimadzu Corporation, Kyoto, Japan). The instrument was calibrated for temperature and heat flow using indium and zinc standards. The samples (2–3 mg) were placed in sealed aluminum pans under nitrogen purge at a flow rate of 30 mL/min. The samples were heated from 100 °C to 220 or 300 °C depending on the melting range of the compound at a heating rate of 10 °C/min. Data acquisition and analysis were performed using the Shimadzu TA-60WS software. Start and end points for the integration of the thermal peak were identified by visual inspection. The amounts of samples were weighed in a Sartorius analytical balance model ME235S (Sartorius AG, Gottingen, Germany), with a resolution of 0.01 mg. Melting points were determined on an Electrothermal 9100 digital melting point instrument (Thermo Fisher Scientific, Essex, UK).

Bellur Atici E, & Karlığa B. (2015). Identification, synthesis and characterization of process related impurities of benidipine hydrochloride, stress-testing/stability studies and HPLC/UPLC method validations. Journal of Pharmaceutical Analysis, 5(4), 256-268.

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Differential Scanning Calorimetry of Powder Samples

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Differential scanning calorimetry (DSC-60, SHIMADZU) with TA-60 WS software was used for the DSC analysis of the RC and CC-PE powder samples. Samples (4–6) mg were placed in aluminum pans and then hermetically sealed. An empty pan was used as the reference. The temperature range for the samples to be heated was (25 to 250) °C and the heating rate was 10 °C/min [30 (link)].

Ali N.A., Dash K.K., Pandey V.K., Tripathi A., Mukarram S.A., Harsányi E, & Kovács B. (2023). Extraction and Encapsulation of Phytocompounds of Poniol Fruit via Co-Crystallization: Physicochemical Properties and Characterization. Molecules, 28(12), 4764.

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Thermal Characterization of Starches

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A differential scanning calorimeter was used to determine the temperature profiles of native starch and modified sago starch (Type DSC-60, Shimadzu Corporation, Kyoto, Japan). Scanning was carried out at a temperature range of 30–200 °C with a scanning speed of 10 °C/minute. An empty pan was used as a reference, and the data were analyzed by TA-60WS software (Shimadzu Corporation, Kyoto, Japan).

Sumardiono S., Jos B., Pudjihastuti I., Yafiz A.M., Rachmasari M, & Cahyono H. (2021). Physicochemical Properties of Sago Ozone Oxidation: The Effect of Reaction Time, Acidity, and Concentration of Starch. Foods, 10(6), 1309.

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Thermal Analysis of Curcumin and Excipients

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DSC thermograms of curcumin, MCC PH102, Aerosil^® and LS-9 were obtained using a DSC-60 instrument equipped with an intra-cooler and controlled by TA-60 WS software (Shimadzu, Kyoto, Japan). Samples were weighed, transferred to hermetically sealed aluminum pans and heated at a rate of 10 °C/min over a range of 0–300 °C. An indium standard was used to calibrate the instrument and enthalpy scale. An inert atmosphere was maintained by purging nitrogen at a rate of 10 mL/min.

Sharma V, & Pathak K. (2016). Effect of hydrogen bond formation/replacement on solubility characteristics, gastric permeation and pharmacokinetics of curcumin by application of powder solution technology. Acta Pharmaceutica Sinica. B, 6(6), 600-613.

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Thermal Analysis of Drug-Excipient Interactions

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The differential scanning thermograms profiles of pure drug, excipients, and physical mixtures thereof were recorded on DSC-60 controlled by TA-60 WS software (Shimadzu, Kyoto, Japan). The samples were weighed and transferred to the equipment for analysis in hermetically sealed aluminium pans. An indium standard was used to calibrate the differential scanning calorimeter temperature. The samples were heated, over a temperature range of 0–300°C. An inert atmosphere was maintained by purging with nitrogen at the flow rate of 20 mL/min.

Sonkar A., Kumar A, & Pathak K. (2016). Cellulose Acetate 398-10 Asymmetric Membrane Capsules for Osmotically Regulated Delivery of Acyclovir. Journal of Pharmaceutics, 2016, 8471520.

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Perimysium Extraction and Denaturation

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Perimysium extraction and denaturation temperature assessment were conducted according to methods described by Vierck et al. (2018) (link) with modifications. Pulverized muscle tissue was homogenized in 0.05 M CaCl₂ using a bead homogenizer (Bead Blaster 24; Benchmark Scientific, Sayreville, NJ). The homogenate was filtered through a 1 mm standard testing sieve (VWR International, Radnor, PA). The perimysial fraction collected on the screen was transferred to a microcentrifuge containing 1X PBS and hydrated for at least 1 h at 4°C prior to peak transitional temperature measurement. Ten milligram of hydrated samples was placed in a hermetic aluminum crucible (S201-53090; Shimadzu, Kyoto, Japan), and the aluminum crucible was sealed using a sealing press (SSC-30; Shimadzu). The sample crucible and a sealed empty crucible, for a reference crucible, were placed at the stage of the differential scanning calorimeter (DSC-60; Shimadzu). The temperature program was set from room temperature to 100°C with a 5°C/min temperature increase. To analyze the data the TA-60WS software (Shimadzu) was used to determine the peak transitional temperature (°C).

Welter A.A., Wu W.J., Maurer R., O’Quinn T.G., Chao M.D., Boyle D.L., Geisbrecht E.R., Hartson S.D., Bowker B.C, & Zhuang H. (2022). An Investigation of the Altered Textural Property in Woody Breast Myopathy Using an Integrative Omics Approach. Frontiers in Physiology, 13, 860868.

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Thermal Behaviour Analysis of Treated and Raw Samples

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The thermal behaviour of the treated and raw samples was studied and compared using differential scanning calorimetry (DSC). The equipment, Shimadzu DSC-60 was operated using TA-60WS software. For analysis, 55 mg of sample was placed in an aluminium pan and an empty pan was used as a reference. The measurements were carried out between 25°C and 500°C with a linear increase of 10°C/min (Ballesteros et al., 2015) .

Ravindran R., Jaiswal S., Abu-Ghannam N, & Jaiswal A.K. (2017). Two-step sequential pretreatment for the enhanced enzymatic hydrolysis of coffee spent waste. Bioresource technology, 239.

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Thermal Behavior Analysis of Treated and Raw Samples

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The thermal behaviour of the treated and raw samples were studied and compared using differential scanning calorimetry (DSC). The equipment, Shimadzu DSC-60 was operated using TA-60WS software. For analysis, 55 mg of sample was places in an aluminium pan and an empty pan was used as a reference. The measurements were carried out between 25°C and 500°C with a linear increase of 10°C/minute (Ballesteros et al., 2015) .

Ravindran R., Jaiswal S., Abu-Ghannam N, & Jaiswal A.K. (2017). Evaluation of ultrasound assisted potassium permanganate pre-treatment of spent coffee waste. Bioresource technology, 224.

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Thermal Behavior of Pretreated SCW

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Differences in the thermal behaviour of SCW after pretreatment was studied using differential scanning calorimetry (DSC), using 55 mg of the pretreated SCW in an aluminium pan with an empty pan used as a reference. The thermograms were obtained by increasing the temperatures from 20°C to 500°C at a rate of 10°C per min at a constant nitrogen atmosphere. All measurements were carried out between 25°C and 500°C with a linear increase of 10°C in a Shimadzu DSC-60 installed with TA-60WS software.

Ravindran R., Sarangapani C., Jaiswal S., Cullen P.J, & Jaiswal A.K. (2017). Ferric chloride assisted plasma pretreatment of lignocellulose. Bioresource technology, 243.

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