The cooling/heating process of the samples was controlled using the FTIR600 SP Linkam stage with T96 LinkPad system controller, available at the University of Warsaw. For structural analysis of the obtained materials, transmission electron microscopy was used: TEM model JEM-1011 (JEOL, Tokyo, Japan) equipped with a model EDS INCA analyzer (Oxford, UK), in the Electron Microscopy Platform, Mossakowski Medical Research Centre, Polish Academy of Science, Warsaw. SAXRD measurements were performed with a Bruker Nanostar system (Cu Kα radiation, parallel beam formed by cross-coupled Goebel mirrors and a 3-pinhole collimation system, VANTEC 2000 area detector, Bruker, Billerica, MA, USA). Spectroscopy measurements in the UV–vis range were performed using GENESYS 50 UV-Vis spectrophotometer (Thermo Fisher Scientific, Waltham, MA, USA), available at the University of Warsaw.
Tem model jem 1011
Manufactured by JEOL
Sourced in Japan
The JEOL JEM-1011 is a transmission electron microscope (TEM) designed for a wide range of applications. It provides high-resolution imaging and analysis capabilities for materials science, life science, and other research fields. The JEM-1011 is equipped with advanced optics and a stable electron source to deliver clear, high-quality images and data.
Automatically generated - may contain errors
Lab products found in correlation
D2 phaser, by Bruker (2 mentions)
Lambda 35 uv vis spectrophotometer, by PerkinElmer (2 mentions)
Nanostar system, by Bruker (1 mentions)
Genesys 50 uv vis spectrophotometer, by Thermo Fisher Scientific (1 mentions)
1000 ft ir spectrometer, by PerkinElmer (1 mentions)
Phi 5600 multi technique xps, by Physical Electronics (1 mentions)
4 protocols using tem model jem 1011
1
Structural Analysis of Nanomaterials
2
Comprehensive Materials Characterization Protocol
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Powder XRD patterns were recorded using
a Bruker diffractometer [Cu Kα (λ = 1.5406 Å) X-ray
source] (D2-Phaser, Bruker, Germany). The phase of TiO2 was confirmed by comparison of major peak positions reported in
standard JCPDS database. SEM, TEM, and energy-dispersive X-ray (EDX)
spectroscopy were carried out on Jeol, JED-2200 series (Akishima,
Tokyo 196-8558, Japan) and Jeol TEM model JEM-1011 (Japan) at 100
keV, respectively. UV spectroscopy was performed on a Lambda 35 UV–Vis
spectrophotometer (PerkinElmer, Waltham, MA, USA) in quartz cuvettes
using distilled water as the reference solvent. The samples were prepared
by diluting 1 mL of the NP reaction solution (collected during and
at the end of the reaction) in 9 mL of water. FT-IR spectra were recorded
on a PerkinElmer Spectrum 100 FT-IR spectrometer (FT-IR, PerkinElmer,
Waltham, MA, USA) in the transmittance mode in the 400–4000
cm–1 range.
a Bruker diffractometer [Cu Kα (λ = 1.5406 Å) X-ray
source] (D2-Phaser, Bruker, Germany). The phase of TiO2 was confirmed by comparison of major peak positions reported in
standard JCPDS database. SEM, TEM, and energy-dispersive X-ray (EDX)
spectroscopy were carried out on Jeol, JED-2200 series (Akishima,
Tokyo 196-8558, Japan) and Jeol TEM model JEM-1011 (Japan) at 100
keV, respectively. UV spectroscopy was performed on a Lambda 35 UV–Vis
spectrophotometer (PerkinElmer, Waltham, MA, USA) in quartz cuvettes
using distilled water as the reference solvent. The samples were prepared
by diluting 1 mL of the NP reaction solution (collected during and
at the end of the reaction) in 9 mL of water. FT-IR spectra were recorded
on a PerkinElmer Spectrum 100 FT-IR spectrometer (FT-IR, PerkinElmer,
Waltham, MA, USA) in the transmittance mode in the 400–4000
cm–1 range.
3
Cardiac and Liver Toxicity Assessment
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Mice were intravenously injected with drugs at 5 mg (as DOX)/kg (body weight) on days 0, 3, 7, 10, 14, 17, and 21. After blood samples and whole hearts were isolated 72 hours after the last injection, serum levels of aspartate aminotransferase (AST) and alanine aminotransferase (ALT) were measured by the core laboratory at the ASAN medical center to monitor liver function, and 10–20 pieces of tissue samples (1×2×2 mm) were taken from the myocardium of the left ventricle. Tissue samples were immediately fixed in 3% (v/v) glutaraldehyde in PBS. Before sectioning, tissue samples were washed with PBS, postfixed in 1% (w/v) osmium tetroxide for 1 hour, and dehydrated by passing through a series of graded ethanol. Then, tissue samples were infiltrated with acetone and poly/bed 812 plastic resin (Ted Pella, Inc., Redding, CA, USA), and embedded in plastic block molds with 100% poly/bed 812. Ultra thin sections (80 nm) were cut from sample block, and mounted on 100 mesh copper grids. Grids were stained with 2% (w/v) uranyl acetate and Reynold’s lead citrate stain. Grids were examined with a TEM model JEM1011 (JEOL).
4
Photocatalyst Characterization Techniques
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The identities of the obtained photocatalysts were confirmed through a number of characterization techniques. Powder XRD patterns were recorded using a Bruker diffractometer (Cu Kα (λ = 1.5406 Å) X-ray source) (D2-Phaser, Bruker, Mannheim, Germany). SEM, TEM, and energy-dispersive X-ray (EDX) spectroscopy were performed on a Jeol, JED-2200 series (Akishima, Tokyo 196-8558, Japan) and a Jeol TEM model JEM-1011 (Japan) at 100 keV, respectively. XPS spectra were measured on a PHI 5600 Multi-Technique XPS (Physical Electronics, Lake Drive East, Chanhassen, MN, USA) using monochromatized Al Ka at 1486.6 eV. Peak fitting was performed using CASA XPS Version 2.3.14 software, Wilmslow, Cheshire, UK. FT-IR analysis was performed for the identification of functional groups on a PerkinElmer, 1000, FT-IR spectrometer, Waltham, MA, USA. The optical study and photocatalytic activity were studied with a Lambda 35 UV–Vis spectrophotometer (PerkinElmer, Waltham, MA, USA) in quartz cuvettes (with a path length of 1 cm) using distilled water as the reference solvent.
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