The largest database of trusted experimental protocols

5 protocols using ethyl acetate acs reagent

1

Calendered Bleached Paper Polymer Blends

Check if the same lab product or an alternative is used in the 5 most similar protocols
In this work, a calendered bleached paper (Advantage MG White High Gloss, Mondi Group, Addlestone, UK) was used, with technical data shown in Table 1, supplied by Serchio Distribuzione (Roma, Italy). According to the technical sheet, the paper is obtained from a long-fiber sulphate pulp. Poly(hexano-6-lactone) (PCL) was purchased from Sigma Aldrich (Taufkirchen, Germany), having average Mw 80,000 g/mol, water content < 0.5%, and melt flow index (160 °C/5 kg) 2.01–4.03. Ethyl acetate (Ethyl acetate—ACS reagent, purity > 99.5%, Mw: 88.11 g/mol) and glycerol (1,2,3-Propanetriol, Glycerin, purity > 99.5%, Mw: 92.09 g/mol) were purchased from Sigma Aldrich (Taufkirchen, Germany). Potato starch (CAS-No 9005-84-9, analytical grade) was purchased from PanReac AppliChem ITW Reagents (Cinisello Balsamo, Milano, Italy); agar-agar was purchased from OXOID, Thermo Fisher Scientific (Rodano, Milano, Italy); polyethylene glycol (PEG) 200 (analytical grade, Density 1.124–1.126 g/cm3, Hydroxyl value: 535–590, Mw~190–210 g/mol; Fluka Analytical, Rodano, Milano, Italy) was used as a plasticizer.
+ Open protocol
+ Expand
2

Polymer Nanoparticle Synthesis and Characterization

Check if the same lab product or an alternative is used in the 5 most similar protocols
The following chemicals were obtained from commercial suppliers and used as received: the polymer poly(d,l-lactic-co-glycolic acid) 50 : 50 (PLGA; MW 38 000–54 000 Da, Tg 46–50 °C), under the commercial name of Resomer® RG 504 was purchased from Boehringer Ingelheim (Ingelheim, Germany) and Evonik Industries (Evonik Röhm GmbH, Germany). Sodium cholate, chloroauric acid (HAuCl4·3H2O), sodium citrate tribasic dehydrate ≥99.0% (Na3C6H5O7·2H2O), PVA (polyvinyl alcohol) MW 85 000–124 000 Da, 97–99% hydrolyzed, taurocholic acid sodium salt hydrate ≥95% (TLC), ethyl acetate ACS reagent, dodecanethiol, phosphotungstic acid hydrate as a contrast agent for microscopy and fluorescent molecule pyrene ≥99.0% were purchased from Sigma Aldrich (St Louis, MO, USA).
+ Open protocol
+ Expand
3

Calendered Bleached Paper Polymer Blends

Check if the same lab product or an alternative is used in the 5 most similar protocols
In this work, a calendered bleached paper (Advantage MG White High Gloss, Mondi Group, Addlestone, UK) was used, with technical data shown in Table 1, supplied by Serchio Distribuzione (Roma, Italy). According to the technical sheet, the paper is obtained from a long-fiber sulphate pulp. Poly(hexano-6-lactone) (PCL) was purchased from Sigma Aldrich (Taufkirchen, Germany), having average Mw 80,000 g/mol, water content < 0.5%, and melt flow index (160 °C/5 kg) 2.01–4.03. Ethyl acetate (Ethyl acetate—ACS reagent, purity > 99.5%, Mw: 88.11 g/mol) and glycerol (1,2,3-Propanetriol, Glycerin, purity > 99.5%, Mw: 92.09 g/mol) were purchased from Sigma Aldrich (Taufkirchen, Germany). Potato starch (CAS-No 9005-84-9, analytical grade) was purchased from PanReac AppliChem ITW Reagents (Cinisello Balsamo, Milano, Italy); agar-agar was purchased from OXOID, Thermo Fisher Scientific (Rodano, Milano, Italy); polyethylene glycol (PEG) 200 (analytical grade, Density 1.124–1.126 g/cm3, Hydroxyl value: 535–590, Mw~190–210 g/mol; Fluka Analytical, Rodano, Milano, Italy) was used as a plasticizer.
+ Open protocol
+ Expand
4

Purification and Characterization of MBQ-167

Check if the same lab product or an alternative is used in the 5 most similar protocols
Two batches (MQ7-PD-025-3 and MQ7QRV-001) of 9-ethyl-3-(5-phenyl-1H-1,2,3-triazol-3-yl)-9H-carbazole (MBQ-167), were received from MBQ Pharma, Inc. Both batches are reported to have a purity of 99.5% as determined by High-Performance Liquid Chromatography (HPLC) analysis. The CAS Registry Number for MBQ-167 is 2097938-73-1. Ethyl acetate ACS reagent (≥99.5%) and heptane ReagentPlus® (99%) were both purchased from Sigma-Aldrich. Ethanol (190 proof) ACS/USP Grade was purchased from Pharmco Aaper. Nanopurified water (18.23 MOhm/cm, pH = 5.98, and mV = 57.3) was obtained from the Aries Filter (Gemini). All reagents were used “as received” without further purification.
+ Open protocol
+ Expand
5

Analytical Extraction Protocol for Organic Compounds

Check if the same lab product or an alternative is used in the 5 most similar protocols
Analytical-grade CA (Mw 30,000), chloroform, acetone, glacial acetic
acid, TMPES (98%), CAT (≥99%), and GA were purchased from Sigma
Aldrich, USA. PEO-b-P4VP (Mw 5000 PEO–20,000
P4VP) was purchased from Polymer Source, Inc., Canada. 190 Proof ethyl
alcohol was purchased from Ultra-Pure, LLC, USA. Visiprep SPE vacuum
manifold DL, Supelclean ENVI-8 SPE Tube bed wt. 500 mg 6 mL, Whatman
qualitative filter paper, ethyl acetate ACS reagent (>99.5%), HCl,
acetonitrile, and 6 mL glass reaction tubes with Teflon were all purchased
from Sigma Aldrich. QuEChERS SpinFiltr dSPE microcentrifuge tubes
(MgSO4, PSA, C18, Cholofiltr) were purchased
from UCT, Inc, USA. Agilent Technologies GC System 7890A coupled with
mass spectrometer inert XL MSD 5975C was used for the analysis of
SPE and SPME samples. SPME experiments were performed using SPME fiber
assembly 50/30 μm DVB/CAR/PDMS Stableflex 24 ga from Supelco
in a standard holder. Nanopure water (NPH2O) from Milli-Q
Direct 16 and Aries FilterWorks Gemini Water Purification Systems
(18.2 MΩ·cm) was used at all times.
+ Open protocol
+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required

Sign up now

Revolutionizing how scientists
search and build protocols!