Xrd 7000 instrument

The Fourier transform infrared (FTIR) spectra were monitored by employing a VERTEX 70 spectrometer (Bruker, Germany). The materials were grounded with KBr (1:100) and then compressed to form tables. The X-ray diffraction (XRD) patterns were collected with a Shimadzu XRD-7000 instrument at a scan rate of 0.02°·S⁻¹ with a 2θ range of 20°–80° and Cu Κα radiation (λ = 0.1542 nm). XPS spectra were obtained via an Escalab 250 Xi spectrometer (Thermo Fisher Scientific Inc., Waltham, MA, USA) with a monochromated source of X-rays (Al Kα, 1486.6 photo energy) as the excitation source. SEM measurements were conducted on a TESCAN MIRA LMS microscope equipped with energy-dispersive X-ray spectrometry (Xplore 30, Oxford, UK). The thermal behavior analyses were conducted in an N₂ atmosphere between room temperature and 800°C at a rate of 10 °C·min⁻¹ using a Q50 thermogravimetric analyzer (TA Instruments- Waters LLC, New Castle, DE, USA). The magnetic properties of the samples were measured using a LakeShore 7404S vibrational sample magnetometer (Lake Shore Cryotronics, Inc., Westerville, OH, USA). The thermal behavior analyses were conducted in an N₂ atmosphere between room temperature and 800°C at a rate of 10 °C·min⁻¹ using a Q50 thermogravimetric analyzer (TA Instruments- Waters LLC, New Castle, DE, USA).

The Fourier transform infrared (FTIR) spectra were monitored by employing a VERTEX 70 spectrometer (Bruker, Germany). The materials were grounded with KBr (1:100) and then compressed to form tables. The X-ray diffraction (XRD) patterns were collected with a Shimadzu XRD-7000 instrument at a scan rate of 0.02°·S⁻¹ with a 2θ range of 20°–80° and Cu Κα radiation (λ = 0.1542 nm). XPS spectra were obtained via an Escalab 250 Xi spectrometer (Thermo Fisher Scientific Inc., Waltham, MA, USA) with a monochromated source of X-rays (Al Kα, 1486.6 photo energy) as the excitation source. SEM measurements were conducted on a TESCAN MIRA LMS microscope equipped with energy-dispersive X-ray spectrometry (Xplore 30, Oxford, UK). The thermal behavior analyses were conducted in an N₂ atmosphere between room temperature and 800°C at a rate of 10 °C·min⁻¹ using a Q50 thermogravimetric analyzer (TA Instruments- Waters LLC, New Castle, DE, USA). The magnetic properties of the samples were measured using a LakeShore 7404S vibrational sample magnetometer (Lake Shore Cryotronics, Inc., Westerville, OH, USA). The thermal behavior analyses were conducted in an N₂ atmosphere between room temperature and 800°C at a rate of 10 °C·min⁻¹ using a Q50 thermogravimetric analyzer (TA Instruments- Waters LLC, New Castle, DE, USA).