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μautolab system type 3

Manufactured by Metrohm

The μAutolab system Type (III) is a potentiostat/galvanostat developed by Metrohm. It provides basic electrochemical measurement capabilities for various applications. The core function of this instrument is to accurately control and measure the potential and current between the working and reference electrodes in an electrochemical cell.

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2 protocols using μautolab system type 3

1

Antioxidant and Anti-radical Evaluation

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A double beam Perkin Elmer UV/Vis/NIR Lambda 19 spectrophotometer (Waltham, MA, USA) was used to measure antioxidant and anti-radical indexes. Standard and reagent blank solutions were located in the sample and reference holders, respectively. QS quartz high performance cuvettes (10 mm optical path) from Hellma Analytics (Jena, Germany) were used.
Electrochemical studies were performed with a μAutolab system Type (III) (EcoChemie, Utrecht, The Netherlands) attached to a 663VA stand (Metrohm, Herisau, Switzerland). In all cases, a conventional cell was used with Ag|AgCl|KCl (3 mol L−1) as the reference electrode, platinum wire as the auxiliary electrode and a screen-printed carbon DRP-110 (Dropsens, Oviedo, Spain) as the working electrode in DPV mode. Data was acquired with a personal computer using the GPES 4.9 software (EcoChemie, Utrecht, The Netherlands).
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2

Penicillamine-Modified Glassy Carbon Electrode

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Stripping measurements were performed in a glass cell by means of a μAutolab System Type III (EcoChemie, The Netherlands) attached to a Metrohm 663 VA Stand (Metrohm, Switzerland) and a personal computer with GPES 4.9 software (EcoChemie).
The reference and the auxiliary electrode were Ag|AgCl|KCl (3 mol L -1 ) and Pt wire, respectively (Metrohm, Switzerland). The working electrode used was a penicillamine-GCE prepared from a commercial glassy carbon disk electrode of 2 mm diameter provided by Metrohm (Switzerland).
A pH meter Basic 20 (Crison Instruments, Barcelona, Spain) was used for pH measurements.
All measurements were carried out at room temperature (20 °C).
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