Resorcinol

Manufactured by Thermo Fisher Scientific

Sourced in United States

Resorcinol is a chemical compound used as a raw material in various industrial applications. It serves as a precursor for the production of other chemicals and materials. Resorcinol has a chemical formula of C₆H₆O₂ and is a white, crystalline solid at room temperature. It is soluble in water and various organic solvents.

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Lab products found in correlation

14 protocols using resorcinol

Synthesis and Characterization of Novel Compounds

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Chemicals and solvents were obtained from Sigma Aldrich (St. Louis, MO, USA) with the exception of resorcinol and 4-bromophenylacetic acid (Acros Organic, Carlsbad,CA, USA), 1,4-dibromobutane (Oakwood Chemical, Estill, SC, USA), sodium iodide (Fisher Scientific, Waltham, MA, USA), and N,N,N’-trimethyl-1,2-ethylenediamine (Toyko Chemical, Tokyo, Japan). Nuclear magnetic resonance spectra were determined in DMSO-d₆ using Varian instruments (¹H, 400; ¹³C, 100Mz; Varian, Inc., Palo Alto, CA, USA). High resolution electrospray ionization (ESI) mass spectra were recorded on a LTQ-Orbitrap Velos mass spectrometer (Thermo Fisher Scientific, Waltham, MA, USA). The FT resolution was set at 100,000 (at 400 m/z). Samples were introduced through direct infusion using a syringe pump with a flow rate of 5 μL/min. Purity was established by combustion analyses performed by Atlantic Microlabs, Inc. (Norcross, GA, USA).

Guo L., Zhang W., Xie Y., Chen X., Olmstead E.E., Lian M., Zhang B., Zaytseva Y.Y., Evers B.M., Spielmann H.P., Liu X., Watt D.S, & Liu C. (2022). Diaminobutoxy-substituted Isoflavonoid (DBI-1) Enhances the Therapeutic Efficacy of GLUT1 inhibitor BAY-876 by Modulating Metabolic Pathways in Colon Cancer Cells. Molecular cancer therapeutics, 21(5), 740-750.

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Resorcinol-Formaldehyde Synthesis Protocol

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Resorcinol (98%, Acros, NJ, USA), formaldehyde (37 wt.% solution in water, Acros, Morris, NJ, USA), isopropanol (99.5%+, Acros, Morris, NJ, USA), acetonitrile (99%+, Acros, Morris, NJ, USA), and HCl (37%, Acros, Morris, NJ, USA), were used as received.

Malkova A.N., Sipyagina N.A., Gozhikova I.O., Dobrovolsky Y.A., Konev D.V., Baranchikov A.E., Ivanova O.S., Ukshe A.E, & Lermontov S.A. (2019). Electrochemical Properties of Carbon Aerogel Electrodes: Dependence on Synthesis Temperature. Molecules, 24(21), 3847.

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Analytical-Grade Chemicals for Research

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Bisphenol A, 4-chlorocatechol
(97%), 4-chloro resorcinol (98%), chloro-p-benzoquinone
(95%), and 4-isobutylacetophenone were purchased from Sigma-Aldrich.
Ibuprofen (99%), 2,4-dichlorophenol (99%), 4-ethylbenzadehyde (98%),
resorcinol (98%), chlorohydroquinone (90%), catechol (99%), and benzoqinone
(99%) were supplied by Acros. Triclosan (99.7%) was from Calbiochem,
and hydroquinone was from Fischer Scientific. Deionized (DI) water
(18.0 mΩ cm) obtained from a Millipore Milli-Q system was used
in all the experiments. All chemicals used in this study were above
analytical grade.

Gou N., Yuan S., Lan J., Gao C., Alshawabkeh A.N, & Gu A.Z. (2014). A Quantitative Toxicogenomics Assay Reveals the Evolution and Nature of Toxicity during the Transformation of Environmental Pollutants. Environmental Science & Technology, 48(15), 8855-8863.

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Synthesis of Metal-Organic Nanomaterials

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Resorcinol (99%), Formaldehyde solution (37% in water), and branched polyethylenimine (MW = 10000) were purchased from Alfa Aesar (Haverhill, MA, USA) and used without any further processing. Cobalt acetylacetonate and nickel acetylacetonate (95%) were obtained from Bean Town Chemicals (Hudson, NH, USA) and used as received. Ethanol proof 200 (VWR) and sodium hydrogen sulfate were purchased from Sigma-Aldrich (St. Louis, MO, USA).

Nabavinia M., Kanjilal B., Fujinuma N., Mugweru A, & Noshadi I. (2021). Developing Eco-Friendly and Cost-Effective Porous Adsorbent for Carbon Dioxide Capture. Molecules, 26(7), 1962.

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Synthesis of Gold Nanoparticles

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Tetrachloroauric acid trihydrate (HAuCl₄·3H₂O, 99.9%), silver nitrate (AgNO₃, 99.99%), resorcinol (99%), N,N,N′,N′-tetramethylguanidine (99%), and potassium silicate (SiO₂ : K₂O 2.5 : 1 wt%, anhydrous) were purchased from Alfa Aesar. BDAC (benzylhexadecyldimethylam-monium chloride, 97%), hexadecyltrimethylammonium bromide (CTAB, 99%, ref. H6269-250G), 8-hydroxyquinoline (99%), sodium borohydride (NaBH₄, 98%), l-ascorbic acid (99%), eriochrome black T, and catechol (98%) were purchased from Sigma-Aldrich. Citric acid monohydrate (99.5%) was purchased from Merck. Powder hexadecyltrimethylammonium chloride (CTAC, 99%) was purchased from Acros Organics. Cellulose tubular membranes (12 kDa) were purchased from Spectra-Por. Milli-Q water with a resistivity above 18.2 MΩ cm was used in all the experiments.

Carone A., Emilsson S., Mariani P., Désert A, & Parola S. (2023). Gold nanoparticle shape dependence of colloidal stability domains. Nanoscale Advances, 5(7), 2017-2026.

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Photocentric UV Laser Resin Synthesis

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The Photocentric UV Laser Hard Clear resin (PUHC resin) was provided by Photocentric 3D. Poly(methyl methacrylate) (MW 120,000), 37 wt% formaldehyde solution in water, ammonium chloride 99.5%, poly(ethylene-alt-maleic anhydride) (Mw 100 kDa – 500 kDa) were purchased from Sigma Aldrich. Anisole (99%), urea (98%) and resorcinol (99%) were purchased from Alfa Aesar. Acetone and sodium hydroxide pellets were purchased from VWR and Fisher Scientific, respectively. All reagents and solvents were used as received. For a detailed description of methods used, please refer to the ESI.

Sanders P., Young A.J., Qin Y., Fancey K.S., Reithofer M.R., Guillet-Nicolas R., Kleitz F., Pamme N, & Chin J.M. (2019). Stereolithographic 3D printing of extrinsically self-healing composites. Scientific Reports, 9, 388.

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Quantification of Sialic Acid in Lung Tissue

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Approximately 1.2 × 1.2 × 1.2 mm pieces from lungs frozen in OCT were thawed and washed 3 times in PBS and the lung piece was weighed. Sample hydrolysis and sialic acid measurement was done following^{90 (link)} using resorcinol (Alfa Aesar), with assays done in 900 µl final volumes. Sialic acid (Vector) was used for standards. Absorbances were measured with a SynergyMX plate reader. Values were then converted to mg sialic acid/g tissue.

Karhadkar T.R., Pilling D., Cox N, & Gomer R.H. (2017). Sialidase inhibitors attenuate pulmonary fibrosis in a mouse model. Scientific Reports, 7, 15069.

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Heterogeneous Catalytic Synthesis Protocol

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As received, ethyl acetoacetate, n-butylamine, resorcinol, acetonitrile, pyridine, cesium nitrate (CsNO₃), ammonium hydroxide (NH₄OH), zirconium oxynitrate (ZrO(NO₃)₂), 12-tungstophosphoric acid (H₃PW₁₂O₄₀:PW), methylene blue (MB), and sulfuric acid (H₂SO₄) were obtained from Alfa Aeser. Both cetyltrimethylammonium bromide (N-cetyl-N,N,N-trimethyl ammonium bromide, CTAB) and tetraethyl orthosilicate (TEOS) were analytical-grade reagents.

Ibrahim A.A., Kospa D.A., Hayes O.R., Khder A.S., El-Hakam S.A, & Ahmed A.I. (2023). Cesium salt of tungstophosphoric acid/mesoporous (zirconia–silica) composite for highly efficient synthesis of 7-hydroxy-4-methyl coumarin and removal of methylene blue. RSC Advances, 13(22), 15243-15260.

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Synthesis of Titanium-based Nanostructures

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A 0.25 mm thick titanium (Ti) foil (99.5%) was commercially sourced from Alfa Aesar (Haverhill, MA, USA). All chemicals used were obtained from commercial suppliers and were employed without the need for further purification. Specifically, hydrochloric acid (HCl, 37%), sodium hydroxide (NaOH, 97%), ethanol (C₂H₅OH, 99%), L-ascorbic acid (C₆H₈O₆, 99%), and rhodamine B (RhB, C₂₈H₃₁ClN₂O₃, 95%) were acquired from Sigma-Aldrich (Steinheim, Germany). (3-Aminopropyl)trimethoxysilane (C₆H₁₇NO₃Si, APTMS, 95%) was acquired from Acros (Renningen, Germany). Resorcinol (C₆H₆O₂, 99%), ammonium hydroxide (NH₄OH, 28%), methylene blue (MB, C₁₆H₁₈ClN₃S, 95%), and silver nitrate (AgNO₃, 99%) were obtained from Alfa Aesar (USA). A formaldehyde solution (CH₂O, 37%) was acquired from Merck (Darmstadt, Germany). De-ionized water with a resistivity exceeding 18.2 MΩ was used to prepare all solutions.

Chang Y.C., Lin I.C., Chin N.C., Juang S.E, & Chou C.M. (2023). Na2Ti3O7@RF@Ag Heterostructures as Efficient Substrates for SERS and Photocatalytic Applications. Molecules, 29(1), 218.

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Synthesis of Graphene Oxide Nanomaterials

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TEOS, EDA, resorcinol, polyvinyl pyrrolidone (PVP), and Triton X-100 were purchased from Alfa Aesar; ethanol, ammonia aqueous solution (28%), formaldehyde, and sodium thiosulfate were supplied by Sinopharm Chemical Reagent Co.; commercial graphene powder was supplied by Deyang Carbonene Technology Co., Ltd.. All reagents were used without purification. GO was synthesized according to the modified Hummers method^{60 (link)}.

Pei F., Lin L., Ou D., Zheng Z., Mo S., Fang X, & Zheng N. (2017). Self-supporting sulfur cathodes enabled by two-dimensional carbon yolk-shell nanosheets for high-energy-density lithium-sulfur batteries. Nature Communications, 8, 482.

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