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2 protocols using 1 1 1 trifluoroacetone

1

Synthesis of Brominated Organic Compounds

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2-Bromobiphenyl and 1,4-dibromobutane were reagent grade and purchased from Fluorochem (Hadfield, UK). n-Butyllithium (BuLi, 2.5 M in hexane), tetrahydrofuran (THF, anhydrous), dichloromethane (DCM), 1,1,1-trifluoroacetone, trifluoromethanesulfonic acid (TFSA), trimethylamine (TMA, 4.2 M in ethanol), poly(vinyl alcohol) (PVA, Mw = 89–98,000, 99% hydrolyzed), polyvinylidene difluoride (PVDF, Mw = 534,000), glutaraldehyde (GA) (50 wt% in water), N-methyl-2-pyrrolidone (NMP), and methanol (anhydrous) were reagent grade and purchased from Sigma-Aldrich (Milano, Italy). All the reagents were used as received.
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2

Synthesis and Characterization of SCECGE

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Ethyl acetate (>99%), acetonitrile (99.9%), 1,1,1-trifluoroacetone (>98%), sodium chloride (99.9%), sodium bicarbonate (99.9%), magnesium sulfate (>99%) and Oxone® potassium monopersulfate compound (CAS no: 70693-62-8) were purchased from Sigma Aldrich, St. Louis, MO, USA. 4-4′-methylene biscyclohexaneamine PACM (99%) were obtained from Air Products, Allentown, PA, USA. SCECGE, was synthesized as previously reported [21 (link)]. All chemicals in this work were used as received.
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