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2 methoxyethylamine

Manufactured by Merck Group

2-methoxyethylamine is a chemical compound used as a laboratory reagent. It is a colorless liquid with a characteristic odor. The compound is commonly used in organic synthesis and as a building block for the production of other chemical substances. Its core function is as a chemical intermediate in various laboratory and industrial processes.

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4 protocols using 2 methoxyethylamine

1

Synthesis and Characterization of Iron Nanoparticles

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Iron tri(acetylacetonate) (2 mmol), 1,2-tetradecanediol (10 mmol), oleic acid (6 mmol), oleylamine (6 mmol), dibenzyl ether, citric acid, diethyl ether, 2-methoxyethylamine, N-(3-Dimethylaminopropyl)-N′-ethylcarbodiimide hydrochloride (EDC), N-Hydroxysuccinimide (NHS), thioglycolic acid, hydroxylamine, and phenanthroline were all purchased from Sigma-Aldrich (St. Louis, Missouri). 1,2-dichlorobenzene and N,N’-dimethylformamide were from Acros Organics (Morris Plains, New Jersey). NH2-PEG (550 Da, 2000 Da, 5000 Da, and 10000 Da) were all obtained from Laysan Bio, Inc. (Arab, Alabama). Slide-A-Lyzer G2 dialysis cassettes, chambered slides, bovine calf serum (BCS) were acquired from Thermo Scientific (Rockford, Illinois). Dulbecco’s Modified Eagle’s Medium (DMEM), Dulbecco’s Phosphate Buffer Saline (DPBS), penicillin, and streptomycin were purchased from Gibco Life Technologies, Inc. (NY, USA).
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2

Synthesis of Phosphazene-Containing Polymers

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PEO (average Mv = 600,000; Sigma-Aldrich) was dried at 50 °C for 24 h under
vacuum before use. Hexachlorocyclotriphosphazene (HCCP, 99%), aluminum
trichloride (AlCl3, 99.9%), 2-methoxyethylamine (99%),
3-methoxypropylamine (99%), n-butyllithium (2.5 M
in hexanes), and anhydrous tetrahydrofuran (THF; 99.9%) were purchased
from Sigma-Aldrich and used without further purification. 2,2,2-Trifluoroethylamine
(98%), Li foil (99.9%), trimethylamine (TEA, 99%), anhydrous acetonitrile
(ACN; 99.8%), and anhydrous dimethyl sulfoxide (DMSO; 99.8%) were
purchased from Fisher Scientific and used as received. LiFePO4 (LFP, 99.5%; Gelon) and Super C45 Carbon Black were dried
at 60 °C before use. All synthesis procedures were carried out
on a Schlenk line under N2, and all other air- and/or moisture-sensitive
procedures were carried out in an Ar-filled glovebox (H2O and O2 less than 1 ppm).
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3

Synthesis of Functionalized Terpyridine Ligands

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Rink amide resin was purchased from Novabiochem; trifluoroacetic acid (TFA), zinc acetate dehydrate and nickel acetate tetrahydrate were purchased from Alfa Aesar; 8-hydroxy-2-quinolinecarbonitrile, (S)-(–)-1-phenylethylamine (Nspe), 4′-chloro-2,2′:6′,2′′-terpyridine and manganese acetate tetrahydrate were purchased from Acros; bromoacetic acid, cobalt acetate tetrahydrate and copper acetate monohydrate were purchased from MERCK; N,N′-diisopropylcarbodiimide (DIC), piperidine, 2-methoxyethylamine, benzylamine, acetonitrile (ACN) and water and HPLC grade solvents were purchased from Sigma-Aldrich; iron perchlorate hydrate was purchased from Strem Chemicals; dimethylformamide (DMF) and methanol (MeOH) solvents were purchased from Bio-Lab Ltd. These reagents and solvents were used without additional purification. 2,2′:6′,2′′-Terpyridine amine (Nterpy) and 8-hydroxy-2-quinolinemethylamine (Nhq) were synthesized according to previously published procedures.13 (link)
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4

Synthesis and Functionalization of Iron Oxide Nanoparticles

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Iron tri(acetylacetonate), 1,2-tetradecanediol, oleic acid, oleylamine, dibenzyl ether, citric acid, diethyl ether, 2-methoxyethylamine, N-(3- Dimethylaminopropyl)-N′-ethylcarbodiimide hydrochloride (EDC), N-Hydroxysuccinimide (NHS), 1,2-dichlorobenzene, and N,N’-dimethylformamide are all purchased from Sigma-Aldrich (St. Louis, Missouri). The LIVE/DEAD Assay kit was purchased from ThermoFisher Scientific (Rockford, Illinois). Human Umbilical Cord Vascular Endothelial Cells (HUVECs) were acquired from Lonza (Portsmouth, New Hampshire). Where it was purchased, HA powder was also purchased from Sigma-Aldrich (St. Louis, Missouri). All functionalized PEG reagents are obtained from Nanocs (Boston, Massachusetts). Slide-A-Lyzer dialysis cassettes are acquired from Thermo Scientific (Rockford, Illinois). Fetal Bovine serum is obtained from Hyclone (Logan, Utah). Media used to culture cells in these experiments is also obtained from Lonza (Portsmouth, New Hampshire).
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