Expression and Purification of VHH Proteins
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Corresponding Organization : Harvard University
Other organizations : Massachusetts General Hospital, Boston Children's Hospital, Imaging Center
Protocol cited in 1 other protocol
Variable analysis
- PDL1 specific VHH A12-
- PDL1 specific VHH B3-
- Irrelevant specificity VHH CTR(1B7)-IFNγ
- Recombinant VHH purity assessed by SDS-PAGE
- Mammalian expression vector pVRC
- HEK293F cells cultured in Freestyle media (ThermoFisher)
- Centrifugation at 8,000 × g for 20 min at 4°C
- Wash buffer: 50 mM Tris, pH 8, 150 mM NaCl and 10 mM imidazole
- Elution buffer: 50 mM Tris, pH 8, 150 mM NaCl, 500 mM imidazole and 10% glycerol
- Size exclusion chromatography on Superdex 200 16/600 column (GE Healthcare) in 50 mM Tris, pH 8, 150 mM NaCl, 10% glycerol
- Amicon 10,000 KDa MWCO filtration unit (Millipore)
- Storage at -80°C
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