Quantification of PAHs by HR-GC-MS

The final extract containing PAHs was spiked with 2 H x -labeled injection standard (d10-acenaphthene, d10-pyrene, d12-benzo[e]pyrene; Wellington Laboratories Inc.). Finally, 2-4 μL was injected to HR-GC-MS (Finnigan MAT 95XP/Agilent Technologies GC 6890N).

Partial Protocol Preview
This section provides a glimpse into the protocol.
The remaining content is hidden due to licensing restrictions, but the full text is available at the following link: Access Free Full Text.

Migdał W., Marcinčák S., Walczycka M., Domagała J., Pluta-Kubica A., Filipczak‐Fiutak M., Migdał A., & Migdał Ł. (2024). Traditional smoking of Wallachian cheeses and sausages in Polish and Slovak parts of the Carpathian Mountains. Journal of Ethnic Foods, 11(1).

Publication 2024

Corresponding Organization :

Other organizations : University of Agriculture in Krakow, University of Veterinary Medicine in Košice

Top 5 similar protocols

Variable analysis

independent variables

Amount of final extract containing PAHs

dependent variables

Detection and measurement of PAHs using HR-GC-MS

control variables

Concentration of 2 H x -labeled injection standard (d10-acenaphthene, d10-pyrene, d12-benzo[e]pyrene)
GC-MS instrument parameters (Finnigan MAT 95XP/Agilent Technologies GC 6890N)

controls

Positive control: 2 H x -labeled injection standard (d10-acenaphthene, d10-pyrene, d12-benzo[e]pyrene)
Negative control: Not explicitly mentioned

Annotations

Based on most similar protocols

Etiam vel ipsum. Morbi facilisis vestibulum nisl. Praesent cursus laoreet felis. Integer adipiscing pretium orci. Nulla facilisi. Quisque posuere bibendum purus. Nulla quam mauris, cursus eget, convallis ac, molestie non, enim. Aliquam congue. Quisque sagittis nonummy sapien. Proin molestie sem vitae urna. Maecenas lorem.

As authors may omit details in methods from publication, our AI will look for missing critical information across the 5 most similar protocols.

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Revolutionizing how scientists
search and build protocols!