Synthesis of Alkyl Halides via Nucleophilic Substitution

1-bromohexane (98%), 1-bromooctane (99%), 1-bromodecane (98%) and 1-bromododecane (95%) were obtained from Sigma-Aldrich Co. (St. Louis, MO, USA). Dimethylamine hydrochloride (99%) was purchased from Acros Organics company (Geel, Belgium). Diethyl ether (99.5%), ethanol (99.8%), acetone (99.5%), sodium hydroxide (99%) and ethyl chloroacetate (99%) were purchased from POCH S.A. (Gliwice, Poland). Deionized water used for synthesis had a specific conductivity not higher than 0.4 μS∙cm⁻¹ at 20 °C.

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Geppert-Rybczyńska M., Mrozek-Wilczkiewicz A., Rawicka P, & Bartczak P. (2024). A Study of the Micellar Formation of N-Alkyl Betaine Ethyl Ester Chlorides Based on the Physicochemical Properties of Their Aqueous Solutions. Molecules, 29(8), 1844.

Publication 2024

1-bromohexane 1-bromooctane 1-bromodecane 1-bromododecane

Corresponding Organization :

Other organizations : University of Silesia in Katowice, Silesian University of Technology

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Variable analysis

independent variables

Concentration of 1-bromohexane (98%)
Concentration of 1-bromooctane (99%)
Concentration of 1-bromodecane (98%)
Concentration of 1-bromododecane (95%)

dependent variables

Not explicitly mentioned

control variables

Purity of dimethylamine hydrochloride (99%)
Purity of diethyl ether (99.5%)
Purity of ethanol (99.8%)
Purity of acetone (99.5%)
Purity of sodium hydroxide (99%)
Purity of ethyl chloroacetate (99%)
Specific conductivity of deionized water (not higher than 0.4 μS·cm^-1 at 20 °C)

positive controls

Not explicitly mentioned

negative controls

Not explicitly mentioned

Annotations

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