Synthesis of Metal Halide Nanocrystals

1-Octadecene (ODE, technical grade, 90%),
potassium thiocyanate (KSCN, 99%) sodium thiocyanate (NaSCN, 98%),
and tin(II) acetate (Sn(OAc)₂) from Sigma-Aldrich; antimony(III)
iodide (SbI₃, 99.9%), bismuth(III) iodide (BiI₃, 99.999%), tin(II) iodide (SnI₂, 99%), tin(II) sulfate
(SnSO₄, 95%), and bismuth(III) chloride (BiCl₃, 99%) from Strem; oleic acid (technical grade, 90%) from Alfa Aesar;
hexanes (99.9%) and methanol (99.9%) from Fisher. All chemicals were
used as received without further purification.

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Roth A.N., Porter A.P., Horger S., Ochoa-Romero K., Guirado G., Rossini A.J, & Vela J. (2024). Lead-Free Semiconductors: Phase-Evolution and Superior Stability of Multinary Tin Chalcohalides. Chemistry of Materials, 36(9), 4542-4552.

Publication 2024

1-Octadecene sodium thiocyanate tin(II) acetate antimony(III)iodide oleic acid hexanes methanol

Corresponding Organization : Ames National Laboratory

Other organizations : Universitat Autònoma de Barcelona

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Variable analysis

independent variables

1-Octadecene (ODE, technical grade, 90%)
Potassium thiocyanate (KSCN, 99%)
Sodium thiocyanate (NaSCN, 98%)
Tin(II) acetate (Sn(OAc)2)
Antimony(III) iodide (SbI3, 99.9%)
Bismuth(III) iodide (BiI3, 99.999%)
Tin(II) iodide (SnI2, 99%)
Tin(II) sulfate (SnSO4, 95%)
Bismuth(III) chloride (BiCl3, 99%)
Oleic acid (technical grade, 90%)

dependent variables

Not explicitly mentioned.

control variables

Hexanes (99.9%)
Methanol (99.9%)

positive controls

None specified.

negative controls

None specified.

Annotations

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