Continuous-wave EPR Spectrometry

Continuous-wave EPR measurements were performed by using a Bruker E500 ElexSys EPR spectrometer and ER4123SHQE X-band cavity resonator as described.^{14 (link)} EPR acquisition parameters: Microwave frequency, 9.45 GHz; microwave power, 0.2 mW; magnetic field modulation, 0.2 mT; modulation frequency, 100 kHz; acquisition number, 4–8 spectra were averaged at each T value.

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Nforneh B, & Warncke K. (2019). Control of Solvent Dynamics around the B12-Dependent Ethanolamine Ammonia-Lyase Enzyme in Frozen Aqueous Solution by using Dimethyl Sulfoxide Modulation of Mesodomain Volume. The journal of physical chemistry. B, 123(26), 5395-5404.

Publication 2019

E500 ElexSys EPR spectrometer X-band cavity resonator

Cavity Magnetic field Microwave

Corresponding Organization : Emory University

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Variable analysis

independent variables

Temperature (T)

dependent variables

EPR signal

control variables

Microwave frequency (9.45 GHz)
Microwave power (0.2 mW)
Magnetic field modulation (0.2 mT)
Modulation frequency (100 kHz)
Acquisition number (4-8 spectra averaged)

controls

No positive or negative controls were explicitly mentioned.

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