Synthesis and Characterization of Calcium Oxalate

Calcium oxalate monohydrate
(COM, CaC₂O₄^.H₂O, 99%,
Alfa Aesar),
sodium oxalate (Na₂C₂O₄, 99%, Sigma-Aldrich),
calcium chloride dihydrate (CaCl₂^.2H₂O, 99%, Sigma-Aldrich), H₂¹⁷O (∼90% ¹⁷O enrichment, CortecNet), H₂¹⁸O (99.3% ¹⁸O enrichment, CortecNet), D₂O (≥99% ²H enrichment, Sigma-Aldrich), and HPLC-grade water (Acros
Organics) were used as received. COD was prepared as previously described
in the literature^{37 (link),41} and stored under vacuum before
any further use.

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Goldberga I., Patris N., Chen C.H., Thomassot E., Trébosc J., Hung I., Gan Z., Berthomieu D., Métro T.X., Bonhomme C., Gervais C, & Laurencin D. (2022). First Direct Insight into the Local Environment and Dynamics of Water Molecules in the Whewellite Mineral Phase: Mechanochemical Isotopic Enrichment and High-Resolution 17O and 2H NMR Analyses. The Journal of Physical Chemistry. C, Nanomaterials and Interfaces, 126(29), 12044-12059.

Publication 2022

Calcium oxalate monohydrate sodium oxalate calcium chloride dihydrate HPLC-grade water

Calcium chloride dihydrate Calcium oxalate monohydrate Hplc Sodium oxalate Vacuum

Corresponding Organization :

Other organizations : Centre National de la Recherche Scientifique, École Nationale Supérieure de Chimie de Montpellier, Université de Montpellier, Institut de Recherche pour le Développement, Laboratoire HydroSciences Montpellier, Université de Lorraine, Institut National de Recherche pour l'Agriculture, l'Alimentation et l'Environnement, École Centrale de Lille, Université d'Artois, Université de Lille, National High Magnetic Field Laboratory, Institut des Biomolécules Max Mousseron, Sorbonne Université

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Variable analysis

independent variables

Calcium oxalate monohydrate (COM, CaC2O4.H2O, 99%, Alfa Aesar)
Sodium oxalate (Na2C2O4, 99%, Sigma-Aldrich)
Calcium chloride dihydrate (CaCl2.2H2O, 99%, Sigma-Aldrich)
H2^17O (∼90% ^17O enrichment, CortecNet)
H2^18O (99.3% ^18O enrichment, CortecNet)
D2O (≥99% ^2H enrichment, Sigma-Aldrich)

dependent variables

Not explicitly mentioned

control variables

HPLC-grade water (Acros Organics)

controls

COD was prepared as previously described in the literature[37,41]
COD was stored under vacuum before any further use

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