NMR and Mass Spectrometry Characterization
Corresponding Organization :
Other organizations : University of Illinois Urbana-Champaign
Variable analysis
- Reagents purchased from Aldrich (Milwaukee, WI)
- Purity of compounds investigated
- NMR spectroscopy at 400 MHz or 500 MHz
- High-resolution mass spectra
- Cellulose thin layer chromatography (TLC) plates visualization
- Varian (Palo Alto, CA) Unity spectrometers used for NMR spectroscopy
- University of Illinois Mass Spectrometry Laboratory used for high-resolution mass spectra
- Iodine or sulphosalicylic acid–ferric chloride stain used for TLC visualization
- Syntheses and characterization of compounds 4–12 described previously in Ref. 30
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