IR-780 iodide (99%), 4-mercaptobenzoic acid (99%), Y2O3 (99.9%), Yb2O3 (99.9%), Er2O3 (99.9%), CF3COONa (99.9%), CF3COOH, 1-octadecene (90%), oleic acid (90%), oleylamine (90%), N,N-dimethylformamide (DMF, anhydrous, 99.8%), and dichloromethane (DCM, AR grade) were all purchased from Sigma-Aldrich and used without further purification. The lanthanide (Ln) trifluoroacetates, Ln(CF3COO)3, were prepared as described in the literature.10 (link)
Protocol detail
Synthesis of Lanthanide-Doped Nanoparticles
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IR-780 iodide
4-mercaptobenzoic acid
Yb2O3
Er2O3
CF3COONa
CF3COOH
1-octadecene
oleic acid
oleylamine
N,N-dimethylformamide
dichloromethane
1 octadecene
4 mercaptobenzoic acid
Dichloromethane
Dimethylformamide
Iodide
Ir 780
Lanthanide
Oleic acid
Oleylamine
Trifluoroacetates
Corresponding Organization : University of Massachusetts Chan Medical School
Other organizations : Dalian University, Dalian University of Technology, Zhejiang University, Pacific Northwest National Laboratory, University of Massachusetts Amherst, Lawrence Berkeley National Laboratory
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Variable analysis
independent variables
- IR-780 iodide (99%)
- 4-mercaptobenzoic acid (99%)
- Y2O3 (99.9%)
- Yb2O3 (99.9%)
- Er2O3 (99.9%)
- CF3COONa (99.9%)
- CF3COOH
- 1-octadecene (90%)
- Oleic acid (90%)
- Oleylamine (90%)
- N,N-dimethylformamide (DMF, anhydrous, 99.8%)
- Dichloromethane (DCM, AR grade)
- Not explicitly mentioned
- Lanthanide (Ln) trifluoroacetates, Ln(CF3COO)3, were prepared as described in the literature.
- Positive control: Not mentioned
- Negative control: Not mentioned
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