Example 13
Re(bpy)(CO)3(OH)
An acetone/water mixed solution (4:3 v/v, 70 mL) containing Re(bpy)(CO)3(OTf) (303 mg, 5.21×10−1 mmol) and potassium hydroxide (1.35 g, 24.1×10 mmol) was heated to reflux overnight. The acetone was slowly distilled off under reduced pressure, and a yellow solid thus separated was filtered off and dried under reduced pressure.
Yield: 120 mg (2.71×10−1 mmol), Yield: 51.5%
Based on most similar protocols
As authors may omit details in methods from publication, our AI will look for missing critical information across the 5 most similar protocols.
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!
