Petroleum ether (60–80 °C, 99%), ethyl acetate (99%), and methanol (99%) were purchased from Loba Chemie Pvt. Ltd. Benzene (99%), toluene (99%), o-xylene (99%), m-xylene (99%), p-xylene (99%), isopropylbenzene (99%), ethylbenzene (99%), mesitylene (99%), zinc chloride (anhydrous, 95%), nitromethane (99%), molecular sieve (4 Å), and silica gel (60–120 mesh) were procured from Spectrochem. Palladium(ii ) acetate (98%), 10% Pd/C, and Amberlyst-15 were procured from Sigma-Aldrich. 5-(Acetoxymethyl)furfural (AcMF) was prepared from fructose following a literature process.28 (link) The solvents were dried over activated molecular sieves for 24 h before use. All the chemicals were used as received without further purification.
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Solvent-Assisted Synthesis of Biomass-Derived Compounds
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Corresponding Organization : National Institute of Technology Karnataka
Other organizations : King Saud University
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Variable analysis
independent variables
- Petroleum ether (60–80 °C, 99%)
- Ethyl acetate (99%)
- Methanol (99%)
- Benzene (99%)
- Toluene (99%)
- O-xylene (99%)
- M-xylene (99%)
- P-xylene (99%)
- Isopropylbenzene (99%)
- Ethylbenzene (99%)
- Mesitylene (99%)
- Zinc chloride (anhydrous, 95%)
- Nitromethane (99%)
- Molecular sieve (4 Å)
- Silica gel (60–120 mesh)
- Palladium(ii) acetate (98%)
- 10% Pd/C
- Amberlyst-15
- 5-(Acetoxymethyl)furfural (AcMF)
- Not explicitly mentioned
- The solvents were dried over activated molecular sieves for 24 h before use.
- All the chemicals were used as received without further purification.
- None specified
- None specified
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