Synthesis of Gold-Palladium Nanoparticles

Pd(acac)₂ (Pd 34.9%, Macklin) and HAuCl₄·3H₂O (99.9%, Aladdin), Chloro(triphenylphosphine)gold(I) (AuPPh₃Cl, 99%, Aladdin), N, N-dimethylformamide (DMF, 99.7%, Macklin), Tetrabutylammonium bromide (TBAB, 99%, Aldrich), Potassium titanium oxalate (C₄H₂K₂OTi, 99%, Macklin), 1, 2-dichloropropane (99%, Macklin), 4-tert-butylpyridine (99%, Macklin), Poly(vinylpyrrolidone) (PVP, ~ 29000, Aldrich), Oleylamine (OM, 70%, Aldrich) and L-ascorbic acid (AA, 99.5%, Aldrich) and Carbon blacks (xc-72c, Macklin) were used. High-purity water (H₂O, 18.3 MΩ cm) was employed for all experiments.

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Xu Y., Wu D., Zhang Q., Rao P., Deng P., Tang M., Li J., Hua Y., Wang C., Zhong S., Jia C., Liu Z., Shen Y., Gu L., Tian X, & Liu Q. (2024). Regulating Au coverage for the direct oxidation of methane to methanol. Nature Communications, 15, 564.

Publication 2024

Oleylamine L-ascorbic acid

Corresponding Organization : Guangdong University of Technology

Other organizations : Hainan University, Institute of Physics, Chinese Academy of Sciences, Hainan Normal University, Hainan Tropical Ocean University

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Variable analysis

independent variables

Pd(acac)_2 (Pd 34.9%, Macklin)
HAuCl_4·3H_2O (99.9%, Aladdin)
Chloro(triphenylphosphine)gold(I) (AuPPh_3Cl, 99%, Aladdin)
N, N-dimethylformamide (DMF, 99.7%, Macklin)
Tetrabutylammonium bromide (TBAB, 99%, Aldrich)
Potassium titanium oxalate (C_4H_2K_2OTi, 99%, Macklin)
1, 2-dichloropropane (99%, Macklin)
4-tert-butylpyridine (99%, Macklin)
Poly(vinylpyrrolidone) (PVP, ~ 29000, Aldrich)
Oleylamine (OM, 70%, Aldrich)
L-ascorbic acid (AA, 99.5%, Aldrich)
Carbon blacks (xc-72c, Macklin)

dependent variables

Not explicitly mentioned

control variables

High-purity water (H_2O, 18.3 MΩ cm)

controls

No positive or negative controls were explicitly mentioned.

Annotations

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