Synthesis and Characterization of Functional Polymers

Butyl methacrylate, 4-cyano-4-(phenocarbonothioylthio)pentanoate, poly(ethylene glycol) methyl ether (M_n = 2,000 Da), dicyclohexylcarbodiimide, 4-dimethylaminopyridine, and dichloromethane were purchased from Sigma-Aldrich. 2-(diethylaminoethyl) methacrylate was purchased from TCI Chemicals. 2,2′-azobis(4-methoxy-2,4-dimethylvaleronitrile) was purchased from Wako Chemicals. Pyridyl disulfide ethyl methacrylate was synthesized as described previously (36, 40 (link)). 2′3′-cGAMP was synthesized as described previously (36 (link)). Alexa Fluor 647 Maleimide was purchased from Thermo Fisher Scientific.

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Florian D.C., Bennett N.E., Odziomek M., Baljon J.J., Wehbe M., Merkel A.R., Fischer M.A., Savona M.R., Rhoades J.A., Guelcher S.A, & Wilson J.T. (2023). Nanoparticle STING Agonist Reprograms the Bone Marrow to an Antitumor Phenotype and Protects Against Bone Destruction. Cancer Research Communications, 3(2), 223-234.

Publication 2023

Butyl methacrylate dicyclohexylcarbodiimide 4-dimethylaminopyridine dichloromethane 2,2′-azobis(4-methoxy-2,4-dimethylvaleronitrile) Alexa Fluor 647 Maleimide

4 dimethylaminopyridine Alexa fluor 647 Butyl methacrylate Cgamp Dichloromethane Dicyclohexylcarbodiimide Diethylaminoethyl methacrylate Disulfide Ethyl methacrylate Ethylene glycol ether Maleimide Pentanoate Poly

Corresponding Organization : VA Tennessee Valley Healthcare System

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Variable analysis

independent variables

Butyl methacrylate
4-cyano-4-(phenocarbonothioylthio)pentanoate
Poly(ethylene glycol) methyl ether (M_n = 2,000 Da)
Dicyclohexylcarbodiimide
4-dimethylaminopyridine
Dichloromethane
2-(diethylaminoethyl) methacrylate
2,2'-azobis(4-methoxy-2,4-dimethylvaleronitrile)
Pyridyl disulfide ethyl methacrylate
2'3'-cGAMP
Alexa Fluor 647 Maleimide

dependent variables

Not explicitly mentioned

control variables

Not explicitly mentioned

positive controls

Not specified

negative controls

Not specified

Annotations

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