Quantitative Proteomics Workflow for E. coli
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Corresponding Organization :
Other organizations : Max Planck Institute of Biochemistry
Protocol cited in 46 other protocols
Variable analysis
- Growth medium (standard LB medium)
- Lysis buffer (4% SDS, 100 mM Tris, pH 8.5)
- Reducing agent (10 mM DTT)
- Alkylating agent (20 mM iodoacetamide)
- Proteases (LysC and trypsin)
- Protein-to-enzyme ratio for UPS1 (12:1) and UPS2 (10:1)
- Growth and harvesting of E. coli K12 strain
- Lysis and shearing of DNA
- Protein extraction and purification
- Protein quantification (tryptophan fluorescence emission assay)
- Peptide purification (C18 Sep Pak cartridge and StageTips)
- Peptide quantification (absorbance at 280 nm)
- Centrifugation conditions (15,000 × g for 15 min)
- Incubation time (30 min for alkylation, 5 h for LysC digestion, overnight for trypsin digestion)
- Dilution factor (1:3 with ammonium bicarbonate buffer)
- Mass spectrometry analysis (Q Exactive)
- Positive control: UPS1 and UPS2 standards
- Negative control: Not explicitly mentioned
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