Synthesis of Phosphorus-Based Nanomaterials

All manipulations were performed under inert atmosphere using Schlenk
techniques. Pd(NO₃)₂·2H₂O, 1-chloro-2-nitrobenzene,
and 1-chloro-3-nitrobenzene were used as received from Sigma-Aldrich.
Ketjen black EC 600JD (surface area = 1400 m²/g) was purchased
from Akzo Nobel. Black phosphorus (bP) was prepared according to the
literature procedure^{17 (link)} and the liquid-phase
exfoliation of bP was performed according to a protocol set up in
our laboratories.^{18 (link)}

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Vanni M., Serrano-Ruiz M., Telesio F., Heun S., Banchelli M., Matteini P., Mio A.M., Nicotra G., Spinella C., Caporali S., Giaccherini A., D’Acapito F., Caporali M, & Peruzzini M. (2019). Black Phosphorus/Palladium Nanohybrid: Unraveling the Nature of P–Pd Interaction and Application in Selective Hydrogenation. Chemistry of Materials, 31(14), 5075-5080.

Publication 2019

Pd(NO3)2·2H2O Ketjen black EC 600JD

1 chloro 2 nitrobenzene Atmosphere Black phosphorus Nitrobenzene

Corresponding Organization : Institute for the Chemistry of OrganoMetallic Compounds

Other organizations : University of Siena, Scuola Normale Superiore, Istituto Nanoscienze, Nello Carrara Institute of Applied Physics, Institute for Microelectronics and Microsystems, University of Florence, European Synchrotron Radiation Facility

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Variable analysis

independent variables

Pd(NO3)2·2H2O
1-chloro-2-nitrobenzene
1-chloro-3-nitrobenzene
Ketjen black EC 600JD
Black phosphorus (bP)

dependent variables

Not explicitly mentioned

control variables

All manipulations were performed under inert atmosphere using Schlenk techniques.

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