The
deuterated solvent (CDCl3)
used for NMR spectroscopy, silica gel 60 (230–400 mesh) for
column chromatography, trifluoroacetic acid, p-chloranil,
MB, DPBF, triethylamine, benzene, acetonitrile, sodium ascorbate,
copper sulfate pentahydrate, cresyl violet, and boron trifluoride
diethyl etherate were provided by Merck. The following chemicals were
obtained from Sigma-Aldrich: ethanol, methanol tetrahydrofuran, sodium
thiosulfate, dimethyl sulfoxide, 2,4-dimethylpyrrole, N,N-dimethylformamide, acetone, dichloromethane,
iodic acid, iodine, hexane, sodium sulfate, N-bromosuccinimide, and glacial acetic acid. n-Butylamine was purchased from Alfa Aesar. The following
chemicals were obtained from Acros Organics: piperidine and 4-hydroxybenzaldehyde.
Bromo-1,8-naphthalic anhydride was purchased from TCI. Zinc phthalocyanine
and 1-azido-1-deoxy-β-d -glucopyranoside tetraacetate
were purchased from ABCR. The rest of the chemicals used in the synthesis
were of reagent grade unless otherwise specified.
deuterated solvent (CDCl3)
used for NMR spectroscopy, silica gel 60 (230–400 mesh) for
column chromatography, trifluoroacetic acid, p-chloranil,
MB, DPBF, triethylamine, benzene, acetonitrile, sodium ascorbate,
copper sulfate pentahydrate, cresyl violet, and boron trifluoride
diethyl etherate were provided by Merck. The following chemicals were
obtained from Sigma-Aldrich: ethanol, methanol tetrahydrofuran, sodium
thiosulfate, dimethyl sulfoxide, 2,4-dimethylpyrrole, N,N-dimethylformamide, acetone, dichloromethane,
iodic acid, iodine, hexane, sodium sulfate, N-bromosuccinimide, and glacial acetic acid. n-Butylamine was purchased from Alfa Aesar. The following
chemicals were obtained from Acros Organics: piperidine and 4-hydroxybenzaldehyde.
Bromo-1,8-naphthalic anhydride was purchased from TCI. Zinc phthalocyanine
and 1-azido-1-deoxy-β-
were purchased from ABCR. The rest of the chemicals used in the synthesis
were of reagent grade unless otherwise specified.
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