Synthesis and Characterization of Dental Monomers

BisGMA (Polysciences, Warrington, PA) and HEMA (Acros Organics, NJ) were used as received without further purification as monomers in dentin adhesives. BMPB was synthesized as reported previously in our laboratory.^{30 (link)} 4-((1,3-Bis(methacryloyloxy)propan-2-yl)oxy)– 2-methylene-4-oxo-butanoic acid (BMPMOB) was synthesized in our laboratory and used as a comonomer (Figure 1). Itaconic anhydride (IAA) and glycerol dimethacrylate (GDMA) were obtained from Sigma-Aldrich (St. Louis, MO). Camphoroquinone (CQ), ethyl-4-(dimethylamino) benzoate (EDMAB), and diphenyliodonium hexafluorophosphate (DPIHP) were obtained from Sigma-Aldrich. All other chemicals were reagent grade and used without further purification.

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Song L., Ye Q., Ge X., Misra A., Laurence J.S., Berrie C.L, & Spencer P. (2014). Synthesis and evaluation of novel dental monomer with branched carboxyl acid group. Journal of biomedical materials research. Part B, Applied biomaterials, 102(7), 1473-1484.

Publication 2014

BisGMA glycerol dimethacrylate diphenyliodonium hexafluorophosphate

Anhydride Benzoate Butanoic acid Camphoroquinone Dentin adhesives Diphenyliodonium hexafluorophosphate Glycerol Hema Methylene

Corresponding Organization : Anhui University

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Variable analysis

independent variables

BisGMA (Polysciences, Warrington, PA)
HEMA (Acros Organics, NJ)
BMPB (synthesized previously in laboratory)
BMPMOB (synthesized in laboratory and used as a comonomer)
Itaconic anhydride (IAA)
Glycerol dimethacrylate (GDMA)

dependent variables

Not explicitly mentioned

control variables

All other chemicals were reagent grade and used without further purification

controls

No positive or negative controls were explicitly mentioned.

Annotations

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