Immunoprecipitation of Alpha-Synuclein from CSF
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Corresponding Organization : Karolinska Institutet
Other organizations : Science for Life Laboratory, Uppsala University, IONICS Mass Spectrometry (Canada), Lund University, Skåne University Hospital, Umeå University
Variable analysis
- Incubation of CSF with protein A/G agarose beads for 2 hours to deplete endogenous immunoglobulins
- Incubation of the obtained solution with antibody recognizing αSN overnight at 4 °C
- Incubation of the sample with protein A/G agarose beads for 6 hours at room temperature
- Elution of the bound proteins from the protein A/G agarose beads using 0.2 M glycine (pH 2.6)
- Volume of CSF (50 mL)
- Phosphate-buffered saline (PBS) buffer (20 mM phosphate, 150 mM NaCl, pH 7.4) used for blocking and washing
- Temperature (4 °C for overnight incubation, room temperature for 6-hour incubation)
- Recombinant αSN
- CSF sample without addition of the primary anti-αSN antibody
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