Lignin Characterization by Nitrobenzene Oxidation
Corresponding Organization :
Other organizations : Luxembourg Institute of Science and Technology, UCLouvain
Protocol cited in 5 other protocols
Variable analysis
- Amount of CWR (10 mg)
- Concentration of NaOH (2 M)
- Volume of nitrobenzene (30 μL)
- Reaction temperature (165 °C)
- Reaction duration (1 hour)
- Lignin characterization
- Nitrobenzene oxidation products
- Hach LT200 system for digestion
- Vanillin-D3 as surrogate standard
- Ethyl acetate for washing and extraction
- Centrifugation for separation
- HCl for pH adjustment (2-3)
- NaCl solution for cleaning
- Na2SO4 for drying
- BSTFA for trimethylsilylation
- HP-5MS column for GC-MS analysis
- Agilent 7890B-5977A GC-MS system
- Salicylic acid-D4 as internal standard
- Positive control: Not specified
- Negative control: Not specified
Annotations
Based on most similar protocols
As authors may omit details in methods from publication, our AI will look for missing critical information across the 5 most similar protocols.
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