Capsules from sixty-five different types of coffee capsules belonging to five different brands (named A to E), together with their relative coffee machines, were purchased on local markets in Parma (Italy) or through online stores during 2016 (23 capsules from brand A; 15 capsules, brand B; 10 capsules, brand C; 10 capsules, brand D; and 7 capsules, brand E). Details on the type of coffee are fully described in reference [7 (link)].
Toluene, 2-methylbutanal, 3-methylbutanal, 2,3,5-trimethylpyrazine, and 1H-pyrrole-2-carbaldehyde were purchased from Sigma-Aldrich (St. Louis, MO, USA).
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