Aliquots of the extracted samples (10 mg/mL) were resolved, centrifuged, filtered, and subjected for the Prep-HPLC Analysis, using Waters 2707 (Waters, Milford, MA, USA) linked with UPLC Sunfire C18 column (5 µm, 10 × 250 mm) (Waters, Milford, MA, USA) with the same parameters and elution conditions described in our recent reports [15 (link),16 (link)].
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