The polymer solutions were prepared by dissolving 2.5 g of PPO powder in 100 mL of each of the following solvents, acquired from Sigma Aldrich (now Merck): benzonitrile (anhydrous, ≥99%), carbon disulfide (anhydrous, ≥99%), chloroform (anhydrous, ≥99%, contained 0.5–1.0% ethanol as a stabilizer), ethyl acetate (anhydrous, ≥99.8%), and p-dioxane (anhydrous, ≥99.8%). The pH of the polymer solutions did not vary intentionally during experiments, and the small variations were caused by the combination of PPO (pH = 4) with the selected solvents having pH values comprised between 4 and 7.
Synthesis and Characterization of PPO Polymer Solutions
The polymer solutions were prepared by dissolving 2.5 g of PPO powder in 100 mL of each of the following solvents, acquired from Sigma Aldrich (now Merck): benzonitrile (anhydrous, ≥99%), carbon disulfide (anhydrous, ≥99%), chloroform (anhydrous, ≥99%, contained 0.5–1.0% ethanol as a stabilizer), ethyl acetate (anhydrous, ≥99.8%), and p-dioxane (anhydrous, ≥99.8%). The pH of the polymer solutions did not vary intentionally during experiments, and the small variations were caused by the combination of PPO (pH = 4) with the selected solvents having pH values comprised between 4 and 7.
Corresponding Organization :
Other organizations : Alexandru Ioan Cuza University
Variable analysis
- Solvents used: benzonitrile, carbon disulfide, chloroform, ethyl acetate, and p-dioxane
- Not explicitly mentioned
- Amount of PPO polymer used: 2.5 g
- Volume of solvents used: 100 mL
- PH of the polymer solutions, which varied slightly (between 4 and 7) due to the combination of PPO (pH = 4) with the selected solvents
- No positive or negative controls were explicitly mentioned in the provided information
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