Synthesis of Multifunctional Compounds

Solvents were purchased from Millipore Sigma and used as received unless otherwise noted. All aqueous solutions were prepared with deionized water. Deuterated solvents were purchased from Cambridge Isotopes Laboratories, Inc. Cambridge Isotope Laboratories, Inc. and used as received. 3,5-dibromobenzoic acid, ethyl-3,5,-dibromoisonicotinate, and poly(ethylene glycol) were purchased from Milipore Sigma. 3-Ethynylpyridine was purchased from AmBeed Inc. Tetrakis(acetonitrile)palladium(II) bis(trifluoromethanesulfonate) was purchased from TCI America.

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Lundberg D.J., Brown C.M., Bobylev E.O., Oldenhuis N.J., Alfaraj Y.S., Zhao J., Kevlishvili I., Kulik H.J, & Johnson J.A. (2024). Nested non-covalent interactions expand the functions of supramolecular polymer networks. Nature Communications, 15, 3951.

Publication 2024

Deuterated solvents

Corresponding Organization : Massachusetts Institute of Technology

Other organizations : University of New Hampshire

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Variable analysis

independent variables

Solvents purchased from Millipore Sigma
Deuterated solvents purchased from Cambridge Isotopes Laboratories, Inc.
3,5-dibromobenzoic acid
Ethyl-3,5,-dibromoisonicotinate
Poly(ethylene glycol)
3-Ethynylpyridine
Tetrakis(acetonitrile)palladium(II) bis(trifluoromethanesulfonate)

dependent variables

Measured outcomes not explicitly mentioned

control variables

All aqueous solutions were prepared with deionized water
Deuterated solvents were used as received

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