Nitrobenzene (0.5 mmol), solvent (4 mL), N2H4·H2O (3–5 mmol) and NCM-T (10–20 mg) were added to a 10 mL round-bottom flask fitted equipped with a reflux condenser, and the mixture was stirred for a certain time at 60 °C–80 °C. After the reaction, nitrobenzene conversion and aniline selectivity were determined via gas chromatography (GC 9790II; flame ionization (FID) detector; HP-5 capillary column; nitrogen as carrier gas).
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Nitrobenzene Reduction to Aniline
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Corresponding Organization : Jilin University of Chemical Technology
Other organizations : Jilin University
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Variable analysis
independent variables
- Nitrobenzene (0.5 mmol)
- Solvent (4 mL)
- N2H4·H2O (3–5 mmol)
- NCM-T (10–20 mg)
- Nitrobenzene conversion
- Aniline selectivity
- Reaction time
- Reaction temperature (60 °C–80 °C)
- No positive or negative controls were explicitly mentioned.
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