MALDITOFMS analysis of the oligosaccharide products released by the LPMO reaction was carried out on a 5800 MALDITOFMS (AB SCIEX) using 5-chloro-2-mercapto-benzothiazole (CMBT) and 2,5-dihydroxybenzoic acid (DHB) as the matrix as previously described [43 (link)]. The MS data acquisition mass range was from m/z 500 to 2500.
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