Synthesis of Thiophene Derivatives

Potassium carbonate (K₂CO₃), sodium bicarbonate (NaHCO₃), and OVS were purchased from Alfa Aesar. 4-Bromobenzoyl bromide, hydrazine monohydrate (NH₂NH₂·H₂O), methanol (MeOH), thiophene (Th), 1,4-dioxane (DO), tetrahydrofuran (THF), acetone, and DMF were procured from Acros. Benzeneboronic acid [PhB(OH)₂], palladium tetrakis(triphenylphosphine) [Pd(PPh₃)₄], copper iodide (CuI), and Et₃N were obtained from Sigma–Aldrich (Darmstadt, Germany).

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Ejaz M., Mohamed M.G., Sharma S.U., Lee J.T., Huang C.F., Chen T, & Kuo S.W. (2022). An Ultrastable Porous Polyhedral Oligomeric Silsesquioxane/Tetraphenylthiophene Hybrid as a High-Performance Electrode for Supercapacitors. Molecules, 27(19), 6238.

Publication 2022

DMF copper iodide (CuI),

Acetone Benzeneboronic acid Bromide Copper Dioxane Hydrazine monohydrate Iodide K2co3 Methanol Nahco3 Palladium Tetrahydrofuran Thiophene Triphenylphosphine

Corresponding Organization : Kaohsiung Medical University

Other organizations : National Chung Hsing University, Chinese Academy of Sciences, Ningbo Institute of Industrial Technology

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Variable analysis

independent variables

Potassium carbonate (K2CO3)
Sodium bicarbonate (NaHCO3)
4-Bromobenzoyl bromide
Hydrazine monohydrate (NH2NH2·H2O)
Thiophene (Th)
Benzeneboronic acid [PhB(OH)2]
Palladium tetrakis(triphenylphosphine) [Pd(PPh3)4]
Copper iodide (CuI)

dependent variables

Measured outcomes not explicitly mentioned

control variables

Methanol (MeOH)
1,4-Dioxane (DO)
Tetrahydrofuran (THF)
Acetone

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