Negative-stain EM Analysis of Bcs Variant
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Corresponding Organization :
Other organizations : Chimie et Biologie des Membranes et des Nanoobjects, Université Paris-Saclay, Institut Européen de Chimie et Biologie, Institut Pasteur, Université Paris Cité, Centre National de la Recherche Scientifique
Variable analysis
- Coexpression of Bcs^His^FL_L339D-L343D variant with BcsD
- Direct visualization of the IMAC elution fraction of the purified Bcs^His^FL variant carrying the cis-filamentation–disruptive L^339D-L^343D double mutation upon coexpression with BcsD
- Concentration of the IMAC-eluted sample (0.01 to 0.02 mg/ml)
- Electron microscope operating at 200 kV accelerating voltage and equipped with a field emission gun and an Eagle 4k × 4k CCD camera
- Nominal defocus range of -1.5 to -3 μm
- Low dose of ~30 electrons/Å
- Pixel size of 1.835 Å^2
- Micrograph contrast transfer function correction performed with Gctf through the cryoSPARC v3 interface
- Autopicking and class averaging performed with cryoSPARC's 'Blob picker' and 2D classification tools
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